Structural rationalization of the phase transition behavior in a solid organic inclusion compound: Bromocyclohexane/thiourea

Palmer B.A.; Kariuki B.M.; Morte-Ródenas A.Harris K.D.M.

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Structural rationalization of the phase transition behavior in a solid organic inclusion compound: Bromocyclohexane/thiourea

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Structural properties of the bromocyclohexane/thiourea inclusion compound have been determined using both single-crystal and powder X-ray diffraction over a range of temperatures above and below a first-order phase transition at 233 K in this material. The results demonstrate marked contrasts to the phase transition behavior in the prototypical cyclohexane/thiourea inclusion compound, demonstrating that relatively small changes in molecular geometry (in this case bromine substitution) can have a profound influence on the structural properties of the low-temperature phase in such materials.

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《Crystal growth & design》 |2012年第2期|577-582|共6页
作者
Palmer B.A.; Kariuki B.M.; Morte-Ródenas A.Harris K.D.M.;
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School of Chemistry, Cardiff University, Park Place, Cardiff CF10 3AT, United Kingdom;

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正文语种英语
中图分类晶体学;
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Structural rationalization of the phase transition behavior in a solid organic inclusion compound: Bromocyclohexane/thiourea

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