Synthesis and selected properties of a new solid solution in the Zn _2FeV _3O _(11)-Mg2FeV _3O _(11) system

Blonska-Tabero A.; Filipek E.; Tabero P.

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Synthesis and selected properties of a new solid solution in the Zn _2FeV _3O _(11)-Mg2FeV _3O _(11) system

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摘要

The binary Zn _2FeV _3O _(11)-Mg2FeV _3O _(11) system has been studied by XRD, DTA, IR, and SEM methods. A new continuous substitution solid solution with the formula Zn2-xMgxFeV3O11 has been obtained by high-temperature synthesis. The DTA investigations were used to choose the heating temperatures as well as for determination of thermal stability of the new triclinic phase. The influence of the degree of Mg2 ion incorporation on the unit cell volume as well as on the position of the IR absorption bands of the solid solution have been determined. The morphology of crystals of the new phase is presented.

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《Journal of thermal analysis and calorimetry》 |2012年第2期|671-676|共6页
作者
Blonska-Tabero A.; Filipek E.; Tabero P.;
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作者单位

Department of Inorganic and Analytical Chemistry, West Pomeranian University of Technology, Al. Piastow 42, 71-065 Szczecin, Poland;

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正文语种英语
中图分类物理化学（理论化学）、化学物理学;
关键词
DTA; IR; Solid solution Zn _2FeV _3O _(11)-Mg2FeV _3O _(11); XRD;

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Synthesis and selected properties of a new solid solution in the Zn _2FeV _3O _(11)-Mg2FeV _3O _(11) system

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