Laser synthesis and crystallization of nanocomposite Si/C/N powder

Pan ZW.; Zhang LT.; Li HL.

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Laser synthesis and crystallization of nanocomposite Si/C/N powder

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Ultrafine preceramic Si/C/N composite powders have been prepared from hexamethyldisilazane (HMDS) by laser-induced gas phase reaction, using a new kind of two-reaction-zone reactor which could efficiently increase laser efficiency and production yield compared with a one-reaction-zone reactor. The as-formed products were nanosized (50-80 nm), amorphous powders containing Si-C and Si-N bonds homogeneously mixed with some excess carbon. The production yield was in the range of 88-120 g/h. Changes of chemical composition and crystallization of the powders during heat treatment at 1350 and 1550 degrees C under nitrogen for 1 h were studied. References: 20

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来源
《Journal of Materials Research》 |1998年第7期|1996-2002|共7页
作者
Pan ZW.; Zhang LT.; Li HL.;
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作者单位

Chinese Acad Sci, Inst Phys, POB 603, Beijing 100080, Peoples R China.;

itt.eduS.K.Mishra, P.A.Keyel, M.J.Hawryluk and N.R.Agostinelli contributed equally to this work;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种英语
中图分类工程材料学;
关键词
Ultrafine particles; Ceramic powders; Composite;

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1. LASER SYNTHESIS OF NANOMETRIC Si/C/O POWDERS FROM AN AEROSOL OF HEXAMETHYLDISILOXANE [J] . Stephane FUSIL, Xavier ARMAND, Nathalie HERLINMichel CAUCHETIER Key engineering materials . 1997,第1期

机译：LASER SYNTHESIS OF NANOMETRIC Si/C/O POWDERS FROM AN AEROSOL OF HEXAMETHYLDISILOXANE
2. ChemInform Abstract: Nanometric Si‐Based Oxide Powders: Synthesis by Laser Spray Pyrolysis and Characterization. [J] . N. HERLIN, X. ARMAND, E. MUSSETH. MARTINENGOM. LUCEM. CAUCHETIER Chem Inform . 1996,第52期

机译：ChemInform Abstract: Nanometric Si‐Based Oxide Powders: Synthesis by Laser Spray Pyrolysis and Characterization.
3. Low-cost high-yield synthesis of nanosize powders of Si-based nitrides and carbides by CO_2 laser induced gas phase reactions [J] . Ya-li Li, Yong Liang, Ke-sheng Xiao Materials Letters . 1995,第2期

机译：Low-cost high-yield synthesis of nanosize powders of Si-based nitrides and carbides by CO_2 laser induced gas phase reactions
4. RF-Powder : Fabrication of 0.15-mm Si-powder resonating at microwave frequencies [C] . Naomi Mura, Yuji Furumura, Katsuhiro Fujino, . -1

机译：RF-Powder：制作在微波频率下共振的0.15mm Si-powder
5. Thermodynamic and Kinetic Modeling of Evolution of Mn-Ni-Si-rich Precipitates in Low-Cu Reactor Pressure Vessel Steels [D] . Ke, Huibin. 2017

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8. Fatigue Tests of CO(sub 2)-Laser, CO(sub 2)-Laser Hydrid and Submerged Arc Welded Butt Joint of RAEX S275 LASER and NVA. Volume 1 [R] . Remes, H. 2003

机译：RaEX s275 LasER和NVa的CO（sub 2）-Laser，CO（sub 2）-Laser Hydrid和埋弧焊对接接头的疲劳试验。第1卷

Laser synthesis and crystallization of nanocomposite Si/C/N powder

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