Crystal growth of Bi_2Sr_2Ca_2Cu_3O_(10+x) and (Bi,Pb)_2Sr_2Ca_2Cu_3O_(10+x) by the KCl flux method

Sergey Lee; Ayako Yamamoto; Setsuko Tajima

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Crystal growth of Bi_2Sr_2Ca_2Cu_3O_(10+x) and (Bi,Pb)_2Sr_2Ca_2Cu_3O_(10+x) by the KCl flux method

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Bi_2Sr_2Ca_2Cu_3O_(10+x) and (Bi,Pb)_2Sr_2Ca_2Cu_3O_(10+x) single crystals with a sharp superconducting transition at T_c = 109 K were grown using a modified KCl flux technique. The crystals show platelike morphology with typical dimensions of 0.5 X 0.5 X 0.002 mm~3 and 0.25 X 0.25 X 0.001 mm~3 for Pb-free and Pb-doped compositions, respectively. The formation of Bi-2212 intergrowth in the crystals is suppressed by utilization of a stable MgO crucible, suppression of the KCl evaporation, and isothermal heat treatment at a temperature close to the melting temperature of the oxide precursor in the flux. Morphology, phase purity, and chemical composition of grown crystals were determined by various analysis methods while the superconducting properties were studied by magnetization and resistivity measurements.

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《Journal of Materials Research》 |2002年第9期|2286-2293|共8页
作者
Sergey Lee; Ayako Yamamoto; Setsuko Tajima;
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作者单位

Superconductivity Research Laboratory, ISTEC, Koto-ku, Tokyo 135-0062, Japan;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种英语
中图分类工程材料学;
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1. ChemInform Abstract: Single Crystals of (Bi, Pb)2Sr2CaCu2Oy Grown by the Flux Method Using KCl as the Flux. [J] . T. SHISHIDO, D. SHINDO, N. TOYOTAK. UKEIT. FUKUDA Chem Inform . 1995,第27期

机译：ChemInform Abstract: Single Crystals of (Bi, Pb)2Sr2CaCu2Oy Grown by the Flux Method Using KCl as the Flux.
2. Magnetic study of texture in multifilamentary (Bi, Pb)_(2)Sr_(2)Ca_(2)Cu_(3)O_(10+x) tapes: Evidence for anisotropic orientation [J] . M. R. Cimberle, C. Ferdeghini, G. Grasso Applied physics letters . 2000,第1期

机译：Magnetic study of texture in multifilamentary (Bi, Pb)_(2)Sr_(2)Ca_(2)Cu_(3)O_(10+x) tapes: Evidence for anisotropic orientation
3. Low-temperature scanning laser microscopy of individual filaments extracted from (Bi, Pb)_(2)Sr_(2)Ca_(2)Cu_(3)O_(10+x) tapes [J] . A. G. Sivakov, A. V. Lukashenko, D. Abraimov Applied physics letters . 2000,第18期

机译：Low-temperature scanning laser microscopy of individual filaments extracted from (Bi, Pb)_(2)Sr_(2)Ca_(2)Cu_(3)O_(10+x) tapes
4. Formation of the Bi_2Sr_2Ca_2Cu_3O_(10) phase with and without Pb substitution [C] . J.-C. Grivel, G. Grasso, A. Erb, European conference on applied superconductivity . 1997

机译：形成Bi_2SR_2CA_2CU_3O_（10）相位，没有PB替换

Crystal growth of Bi_2Sr_2Ca_2Cu_3O_(10+x) and (Bi,Pb)_2Sr_2Ca_2Cu_3O_(10+x) by the KCl flux method

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