Crystal structure of (3,5-dimethyl-1H-pyrrol-2-yl)di­phenyl­phosphine oxide

Kang S.K.; Choi E.M.; Son K.

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Crystal structure of (3,5-dimethyl-1H-pyrrol-2-yl)diphenylphosphine oxide

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The title compound, C18H18NOP, was obtained during a search for new P,N-containing ligands with the potential to generate precatalysts with chromium(III) for selective ethylene oligomerization. In the crystal, mutual pairs of N—H⋯O=P hydrogen bonds link two molecules into a dimer with individual molecules related by a twofold rotation axis. The P=O bond length of 1.4740 (15) Å is not elongated although the O atom is involved in hydrogen bonding. The crystal structure is further stabilized by van der Waals interactions between the dimers, linking the molecules into a three-dimensional network structure.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2017年第8期|1268-1270|共3页
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Kang S.K.; Choi E.M.; Son K.;
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Crystal structure of (3,5-dimethyl-1H-pyrrol-2-yl)di­phenyl­phosphine oxide

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Crystal structure of (3,5-dimethyl-1H-pyrrol-2-yl)diphenylphosphine oxide