Ethyl 2-(4-meth­oxy­phen­yl)-6-oxa-3-aza­bicyclo3.1.0hexane-3-carboxyl­ate: crystal structure and Hirshfeld analysis

Zukerman-Schpector J.; Sugiyama F.H.; Garcia A.L.L.Correia C.R.D.Jotani M.M.Tiekink E.R.T.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Ethyl 2-(4-methoxyphenyl)-6-oxa-3-azabicyclo3.1.0hexane-3-carboxylate: crystal structure and Hirshfeld analysis

【24h】

Ethyl 2-(4-methoxyphenyl)-6-oxa-3-azabicyclo3.1.0hexane-3-carboxylate: crystal structure and Hirshfeld analysis

机译：

获取原文

获取原文并翻译 | 示例

掌桥外文数据库（机构版） >>

开具论文收录证明 >>

文献代查 >>

页面导航

摘要
著录项
相似文献
相关主题

摘要

The title compound, C14H17NO4, features an epoxide-O atom fused to a pyrrolidyl ring, the latter having an envelope conformation with the N atom being the flap. The 4-methoxyphenyl group is orthogonal to dihedral angle = 85.02 (6)° and lies to the opposite side of the five-membered ring to the epoxide O atom, while the N-bound ethyl ester group (r.m.s. deviation of the five fitted atoms = 0.0187 Å) is twisted with respect to the ring dihedral angle = 17.23 (9)°. The most prominent interactions in the crystal are of the type methine-C—H⋯O(carbonyl) and these lead to the formation of linear supramolecular chains along the c axis; weak benzene-C—H⋯O(epoxide) and methine-C—H⋯O(methoxy) interactions connect these into a three-dimensional architecture. The analysis of the Hirshfeld surface confirms the presence of C—H⋯O interactions in the crystal, but also the dominance of H⋯H dispersion contacts.

著录项

来源
《Acta Crystallographica Section E: Crystallographic Communications》 |2017年第8期|1218-1222|共5页
作者
Zukerman-Schpector J.; Sugiyama F.H.; Garcia A.L.L.Correia C.R.D.Jotani M.M.Tiekink E.R.T.;
展开▼
作者单位

展开▼
收录信息
原文格式 PDF
正文语种英语
中图分类
关键词

相似文献

外文文献
中文文献
专利

1. 2-[1-(4-Bromophenyl)-3-hydroxy-3-(4-methoxyphenyl)propyl]cyclohexanol [J] . #199, elik #205, ., Acta Crystallographica Section E: Crystallographic Communications . 2013,第7期

机译：2-[1-(4-Bromophenyl)-3-hydroxy-3-(4-methoxyphenyl)propyl]cyclohexanol
2. 5-{2-(4-Chlorophenyl)-1-[2-(4-chlorophenyl)-1-(3,4,5-trimethoxyphenyl)ethoxy]ethyl}-1,2,3-trimethoxybenzene [J] . Fu Y., Hou H., Hu X., Acta Crystallographica Section E: Crystallographic Communications . 2012,第4期

机译：5-{2-(4-Chlorophenyl)-1-[2-(4-chlorophenyl)-1-(3,4,5-trimethoxyphenyl)ethoxy]ethyl}-1,2,3-trimethoxybenzene
3. Synthesis, Crystal Structure and Hirshfeld Surface Analysis of Ethyl 4-(4-(2-Bromoethyl)-1H-1,2,3-triazol-1-yl)benzoate [J] . Gokturk T., Hokelek T., Gup R. Crystallography reports . 2021,第6期

机译：Synthesis, Crystal Structure and Hirshfeld Surface Analysis of Ethyl 4-(4-(2-Bromoethyl)-1H-1,2,3-triazol-1-yl)benzoate
4. 5-{2-(4-Chlorophenyl)-1-2-(4-chlorophenyl)-1-(345-trimethoxyphenyl)ethoxyethyl}-123-trimethoxybenzene [O] . Ying Fu, Mu Yuan, Xuemei Hu, 2012

机译：5-{2-(4-Chlorophenyl)-1-2-(4-chlorophenyl)-1-(345-trimethoxyphenyl)ethoxyethyl}-123-trimethoxybenzene
5. 5-{2-(4-Chlorophenyl)-1-[2-(4-chlorophenyl)-1-(3,4,5-trimethoxyphenyl)ethoxy]ethyl}-1,2,3-trimethoxybenzene [O] . Fu, Ying, Yuan, Mu, Hu, Xuemei, 2012

机译：5-{2-(4-Chlorophenyl)-1-[2-(4-chlorophenyl)-1-(3,4,5-trimethoxyphenyl)ethoxy]ethyl}-1,2,3-trimethoxybenzene

Ethyl 2-(4-meth­oxy­phen­yl)-6-oxa-3-aza­bicyclo3.1.0hexane-3-carboxyl­ate: crystal structure and Hirshfeld analysis

摘要

著录项

相似文献

相关主题

期刊订阅

Ethyl 2-(4-methoxyphenyl)-6-oxa-3-azabicyclo3.1.0hexane-3-carboxylate: crystal structure and Hirshfeld analysis