Synthesis and crystal structure of N-(4-chloro­phen­yl)-5,7-dimethyl-1,2,4-triazolo1,5-apyrimidin-2-amine

Repich H.; Orysyk S.; Savytskyi P.Pekhnyo V.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Synthesis and crystal structure of N-(4-chlorophenyl)-5,7-dimethyl-1,2,4-triazolo1,5-apyrimidin-2-amine

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Synthesis and crystal structure of N-(4-chlorophenyl)-5,7-dimethyl-1,2,4-triazolo1,5-apyrimidin-2-amine

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The title compound, C13H12ClN5, was synthesized by the cyclization of 1-(4,6-dimethylpyrimidin-2-yl)-4-phenylthiosemicarbazide in the presence of Ni(NO3)2. The molecular structure of the compound is essentially planar. In the crystal, molecules form dimers via pairs of N—H⋯N hydrogen bonds between the H atom of the exocyclic amino group and the N atom at the 4-position of the triazole ring. The resulting dimers are packed into layers which are connected by π-stacking interactions between the aromatic systems of the pyrimidine and benzene nuclei, and between the triazole cores.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2017年第1期|35-37|共3页
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Repich H.; Orysyk S.; Savytskyi P.Pekhnyo V.;
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Synthesis and crystal structure of N-(4-chloro­phen­yl)-5,7-dimethyl-1,2,4-triazolo1,5-apyrimidin-2-amine

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Synthesis and crystal structure of N-(4-chlorophenyl)-5,7-dimethyl-1,2,4-triazolo1,5-apyrimidin-2-amine