Crystal structure of catena-polycopper(II)-#956;2-salicylato-diaqua#173;copper(II)-#956;2-salicylato dihydrate

Horn J.A. van der; Lutz M.

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Crystal structure of catena-polycopper(II)-#956;2-salicylato-diaqua#173;copper(II)-#956;2-salicylato dihydrate

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The title compound, {Cu2(C7H4O3)2(H2O)2#183;2H2O}n, contains two copper(II) cations in special positions (one on a twofold rotation axis and one on an inversion centre) and the the salicylate ligand in its dianionic form. By four- and six-coordinate metal coordination, chains are formed parallel to 001, which are extended by O#8212;H#8943;O hydrogen bonding into sheets extending parallel to (100). These sheets are weakly connected by O#8212;H#8943;O hydrogen bonding via the non-coordinating lattice water mol#173;ecules into a three-dimensional network.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2017年第2期|235-238|共4页
作者
Horn J.A. van der; Lutz M.;
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作者单位

Bijvoet Center for Biomolecular Research, Crystal and Structural Chemistry, Faculty of Science, Utrecht University, Padualaan 8, 3584 CH Utrecht, The Netherlands;

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正文语种英语
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关键词
CRYSTAL STRUCTURE; COPPER; SALICYLATE; HYDROGEN BONDING;

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2. Copper(II) complexes of schiff bases derived of 2-hydroxy-3-naphthaldehyde. The crystal and molecular structures of bis-{(phenyl)(2-oxo-3H-naphth-3-ylidene)methylaminato}copper(II) and bis-{(benzene-4-trifluoromethyl)(2-oxo-3H-naphth-3-ylidene)-methylaminato}copper(II) [J] . J.M.Fernández, J.J.Lembrino-Canales, R.Villena Monatshefte fur Chemie . 1994,第3期

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4. Crystal Structure Determination by Crystallographic Image Processing: II. Ccompensate for defocus, astigmatism and crystal tilt [C] . X.D. Zou NATO advanced study institute on electron crystallography . 1997

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5. Solution based studies of tetranuclear (mu(4)-oxo)-copper(II) complexes. [D] . Birtles, John. 2004

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6. Crystal structure of {2-methyl-2-(pyridin-2-ylmethyl)aminopropan-1-ol-κ3NN′O}bis(nitrato-κO)copper(II) from synchrotron data [O] . Jong Won Shin, Dae-Woong Kim, Jae-Woo Jeon, 2019

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7. Crystal structure of catena-poly[[copper(II)-μ2-salicylato-[diaquacopper(II)]-μ2-salicylato] dihydrate] [O] . Jitschaq A. van der Horn, Martin Lutz 2017

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Crystal structure of catena-polycopper(II)-#956;2-salicylato-diaqua#173;copper(II)-#956;2-salicylato dihydrate

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