A novel one-pot pseudo-five-component condensation reaction towards bifunctional diazepine-tetrazole containing compounds: Synthesis of 1H-tetrazolyl-1H-1,4-diazepine-2,3-dicarbonitriles and 1H-tetrazolyl-benzo[b][1, 4]diazepines

Mofakham H.; Shaabani A.; Mousavifaraz S.; Hajishaabanha F.; Shaabani S.; Ng S.W.

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A novel one-pot pseudo-five-component condensation reaction towards bifunctional diazepine-tetrazole containing compounds: Synthesis of 1H-tetrazolyl-1H-1,4-diazepine-2,3-dicarbonitriles and 1H-tetrazolyl-benzo[b][1, 4]diazepines

机译：一种新型的含双官能二氮杂-四唑化合物的一锅假五组分缩合反应：1H-四唑-1H-1,4-二氮杂-2,3-二碳腈和1H-四唑-苯并[b] [1]的合成，4]二氮杂s

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A novel and efficient method has been developed for the one-pot synthesis of bifunctional diazepine-tetrazole containing compounds. 1H-Tetrazolyl-1H-1,4- diazepine-2, 3-dicarbonitrile and 1H-tetrazolyl-benzo[b][1,4]diazepine derivatives were synthesized in good yields using 2,3-diaminomaleonitrile or an aromatic diamine, ketones, trimethylsilyl azide, and an isocyanide in the presence of p-toluenesulfonic acid as a catalyst in methanol at room temperature.

机译：已经开发了一种新颖且有效的方法，用于一锅合成含双功能二氮杂-四唑的化合物。使用2,3-二氨基马来腈或芳香族二胺，酮以高收率合成了1H-四唑-1H-1,4-二氮杂-2、3-二腈和1H-四唑-苯并[b] [1,4]二氮杂衍生物在室温下在甲醇中以对甲苯磺酸为催化剂存在下，将三甲基硅烷基叠氮化物，三甲基硅烷基叠氮化物和异氰酸酯作为催化剂。

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《Molecular diversity》 |2012年第2期|共6页
作者
Mofakham H.; Shaabani A.; Mousavifaraz S.; Hajishaabanha F.; Shaabani S.; Ng S.W.;
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正文语种 eng
中图分类分子物理学、原子物理学;
关键词
1H-Tetrazolyl-1H-1; 4-diazepine-2; 3-dicarbonitrile; 1H-Tetrazolyl-benzob1; 4diazepine; Isocyanide; MCR; Multicomponent reaction; Trimethylsilyl azide;

机译：1H-四唑基-1H-1;4-二氮杂-2;3-二腈;1H-四唑基-苯并[b] [1;4]二氮杂;异氰酸酯;MCR;多组分反应;叠氮化三甲基硅;

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1. A novel one-pot pseudo-five-component condensation reaction towards bifunctional diazepine-tetrazole containing compounds: synthesis of 1H-tetrazolyl-1H-1,4-diazepine-2,3-dicarbonitriles and 1H-tetrazolyl-benzo[b][1,4]diazepines [J] . Hamid Mofakham, Ahmad Shaabani, Sajjad Mousavifaraz, Molecular Diversity . 2012,第2期

机译：一种新型的含双官能二氮杂-四唑的化合物的一锅式伪五组分缩合反应：1H-四唑基-1H-1,4-二氮杂-2,3-二碳腈和1H-四唑基-苯并[b] [1]的合成，4]二氮杂s
2. A Two-Step Synthesis of 1H-Tetrazolyl-1H-1,4-benzonitriles and 1H-Tetrazolyl-benzo [b] [1,4] diazepines [J] . Ahmad Shaabani, Hamid Mofakham, Sajjad Mousavifaraz Synlett . 2012,第5期

机译：1H-四唑基-1H-1,4-苄腈和1H-四唑基苯并[b] [1,4]二氮杂苯的两步合成
3. 5,7-Bis(2'-arylethenyl)-6H-1,4-diazepine-2,3-dicarbonitriles: synthesis, and experimental and theoretical evaluation of the effects of substituents at 5,6,7-positions on the molecular configuration and spectral properties [J] . Pavel A. Tarakanov, Anton O. Simakov, Alexander V. Dzuban, Organic & biomolecular chemistry . 2016,第3期

机译：5,7-双（2'-芳基乙烯基）-6H-1,4-二氮杂-2,3-二碳腈：合成以及5、6、7位取代基对分子构型的影响的实验和理论评估和光谱特性
4. One-pot synthesis of azetidine-2,4-diones via multicomponent reaction of an amine, an acetylenic compound, and an arylsulfonyl isocyanate [C] . Atieh Rezvanian, Abdolali Alizadeh European Symposium on Organic Chemistry . 2009

机译：通过胺，乙酰烯烯化合物和芳基磺基异氰酸酯的多组分反应的氮丁胺-2,4-二乙醚的单壶合成
5. Synthesis of new calix[4]arenes and calix[4]naphthalenes via Sonogashira reactions, photochemically -induced reactions and [2+2] fragment condensation reactions [D] . Al-Saraierh, Hassan 2007

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6. One-Pot Synthesis of Spiro-isobenzofuran Compounds via the Sequential Condensation/Oxidation Reaction of Ninhydrinwith 4-Amino-12-naphthoquinones/2-Amino-14-naphthoquinonesunder Mild Conditions [O] . SeyedehHekmat Mousavi, Mohammad Reza Mohammadizadeh, Zohreh Roshan, 2020

机译：通过茚三酮的顺序缩合/氧化反应的单壶合成螺二苯脲化合物用4氨基-12-萘醌/ 2-氨基-14-萘醌在温和的条件下
7. Ferrocene-Functionalized Dithiocarbamate Zinc(II) Complexes as Efficient Bifunctional Catalysts for the One-Pot Synthesis of Chromene and Imidazopyrimidine Derivatives via Knoevenagel Condensation Reaction [O] . -1

机译：二茂铁 - 官能化二硫代氨基甲酸锌（II）作为通过KNOEVENAGEL缩合反应的单罐合成铬烯和咪唑酰胺衍生物的高效双官能催化剂的复合物

A novel one-pot pseudo-five-component condensation reaction towards bifunctional diazepine-tetrazole containing compounds: Synthesis of 1H-tetrazolyl-1H-1,4-diazepine-2,3-dicarbonitriles and 1H-tetrazolyl-benzo[b][1, 4]diazepines

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