Crystal structure of 5-butyl#173;amino-3-methyl-1-(pyridin-2-yl)-1H-pyrazole-4-carbaldehyde obtained from a microwave-assisted reaction using caesium carbonate as catalyst

Mac#237; as M.A.; Orrego-Hern#225ndez J.Portilla J.

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Crystal structure of 5-butyl#173;amino-3-methyl-1-(pyridin-2-yl)-1H-pyrazole-4-carbaldehyde obtained from a microwave-assisted reaction using caesium carbonate as catalyst

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The title compound, C14H18N4O, synthesized from an unconventional microwave-assisted method using caesium carbonate as catalyst, has an approximately planar conformation with the pyridyl and pyrazole rings inclined by a dihedral angle of 7.94#8197;(3)#176;, allowing the formation of an intra#173;molecular N#8212;H#8943;N hydrogen bond. The supra#173;molecular assembly has a three-dimensional arrangement controlled mainly by weak C#8212;H#8943;O and C#8212;H#8943;#960; inter#173;actions.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2016年第11期|1672-1674|共3页
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Mac#237; as M.A.; Orrego-Hern#225ndez J.Portilla J.;
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Crystal structure of 5-butyl#173;amino-3-methyl-1-(pyridin-2-yl)-1H-pyrazole-4-carbaldehyde obtained from a microwave-assisted reaction using caesium carbonate as catalyst

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