Crystal structure of (2,2′-bi­pyridine-κ2N,N′)bis­(3,5-di-tert-butyl-o-benzo­quinonato-κ2O,O′)ruthenium(II)

Faizi M.S.H.; Ali A.; Potaskalov V.A.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Crystal structure of (2,2′-bipyridine-κ2N,N′)bis(3,5-di-tert-butyl-o-benzoquinonato-κ2O,O′)ruthenium(II)

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Crystal structure of (2,2′-bipyridine-κ2N,N′)bis(3,5-di-tert-butyl-o-benzoquinonato-κ2O,O′)ruthenium(II)

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In the title mononuclear complex, Ru(C14H20O2)2(C10H8N2), the RuII ion has a distorted octahedral coordination environment defined by two N atoms of the chelating 2,2′-bipyridine ligand and four O atoms from two 3,5-di-tert-butyl-o-benzoquinone ligands. In the crystal, the complex molecules are linked by intermolecular C—H⋯O hydrogen bonds and π–π stacking interactions between the 2,2′-bipyridine ligands centroid–centroid distance = 3.538 (3) Å, resulting in a layer structure extending parallel to the ab plane.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2017年第3期|459-462|共4页
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Faizi M.S.H.; Ali A.; Potaskalov V.A.;
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1. ChemInform Abstract: Ruthenium(II) Compounds Containing a Novel Strong π‐Accepting Ligand, 5,5′‐Dimethyl‐2,2′‐bi‐1,3,4‐thiadiazole (dbtd). Crystal Structure of (Ru(bipy)2(dbtd))(PF6)2×Me2CO (bipy: 2,2′‐ bipyridine). [J] . B. D. J. R. FENNEMA, R. A. G. DE GRAAFF, R. HAGEJ. G. HAASNOOTJ. REEDIJKJ. G. VOS Chem Inform . 1991,第26期

机译：ChemInform Abstract: Ruthenium(II) Compounds Containing a Novel Strong π‐Accepting Ligand, 5,5′‐Dimethyl‐2,2′‐bi‐1,3,4‐thiadiazole (dbtd). Crystal Structure of (Ru(bipy)2(dbtd))(PF6)2×Me2CO (bipy: 2,2′‐ bipyridine).
2. Bis(2,2′-bipyridyl)-1κ2N,N′;3κ2N,N′-bis(4-bromo-2-formylphenolato)-1κ2O,O′;3κ2O,O′-bis[μ-2-(5-bromo-2-oxidobenzylideneamino)ethanesulfonato]-1:2κ3O:N,O2;2:3κ3N,O2:O-tricopper(II) monohydrate [J] . Zhang L. Acta Crystallographica Section E: Crystallographic Communications . 2009,第5期

机译：双（2,2'-联吡啶）-1κ2N，N';3κ2N，N'-双（4-溴-2-甲酰基苯酚基）-1κ2O，O';3κ2O，O'-bis [μ-2-（5-溴-2-氧化苄叉亚氨基）乙磺酸盐] -1：2κ3O：N，O2; 2：3κ3N，O2：O-tricopper（II）一水合物
3. Structure ofcis‐bis(4‐allyl‐4H‐1,2,4‐triazole)bis(2,2'‐bipyridine)ruthenium(II) bis(hexafluorophosphate) [J] . Z.‐S. Hu, Y.‐H. Lin, S.‐C. JinJ. G. Vos Acta Crystallographica. Sect.C, Section C. Crystal Structure Communications . 1989,第10期

机译：Structure ofcis‐bis(4‐allyl‐4H‐1,2,4‐triazole)bis(2,2'‐bipyridine)ruthenium(II) bis(hexafluorophosphate)
4. ALKYLATION OF 2,2'-(2,2'-BIPYRIDINE-6,6'-DIYL)BIS-PHENOLATO-N,N',O,ONICKEL(II) [C] . Danielle M.Goken, Dennis G.Peters The Meeting of the Electrochemical Society . 2003

机译：2,2' - （2,2'-Bi0吡啶 -6,6'-二基）双-酚酸盐 -N，N'，O，O镍（II）的烷基化
5. Synthesis and Characterization of [Ru(tpyOH)(bpy)(H2O)][OTf]2 (tpyOH = 4′-Hydroxy-2,2’:6′, 2″- Terpyridine, Bpy = 2,2′-Bipyridine) for Water Oxidation Catalysis [D] . Isaacs, Diane Pearl. 2019

机译：[Ru（TPYOH）（BPY）（H2O）] [otf] 2（TPYOH = 4'-羟基-2,2'：6'，2“ - Terpyridine，BPy = 2,2'- Bi吡啶）的合成与表征用于水氧化催化
6. {μ2-1,4-Bis[2-(4-pyridyl)ethenyl]benzene-κ2N:N′}bis[bis(acetylacetonato-κ2O,O′)copper(II)] [O] . Fang-Fang Jian, Jing Wang, Jing Zhang 2016

机译：{μ2-1,4-双[2-（4-吡啶基）乙炔基]苯-κ2N：N'} bis [bis（乙酰丙酮-κ2O，O'）铜（II）]
7. Bis(2,2′-bipyridyl)-1κ2N,N′;3κ2N,N′-bis(4-bromo-2-formylphenolato)-1κ2O,O′;3κ2O,O′-bis[μ-2-(5-bromo-2-oxidobenzylideneamino)ethanesulfonato]-1:2κ3O:N,O2;2:3κ3N,O2:O-tricopper(II) monohydrate [O] . Ling Zhang 2009

机译：Bis（2,2＆＃8242; -bipyridyl）-1＆＃954; 2N，N＆＃8242 ;; 3＆＃954; 2N，N＆＃8242; -bis（4-bromo-2-formylphenolato）-1＆＃954; 2O ，O＆＃8242 ；； 3＆＃954； 2O，O＆＃8242；-双[＆＃956； -2-（5-溴-2-氧化苄基亚氨基氨基）乙磺酸钠] -1：2＆＃954； 3O：N，O 2； N，O 2。 2：3＆＃954; 3N，O2：一水合O-tricopper（II）
8. Kinetics and Mechanism for the Basic Hydrolysis of BIS (2,2-Dinitropropyl) Acetal (BDNPA) and BIS (2,2-Dinitropropyl) Formal (BDNPF) [R] . Hoffsommer, J. C. 1985

机译：BIs（2,2-二硝基丙基）缩醛（BDNpa）和BIs（2,2-二硝基丙基）甲醛（BDNpF）碱性水解的动力学和机理

Crystal structure of (2,2′-bi­pyridine-κ2N,N′)bis­(3,5-di-tert-butyl-o-benzo­quinonato-κ2O,O′)ruthenium(II)

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Crystal structure of (2,2′-bipyridine-κ2N,N′)bis(3,5-di-tert-butyl-o-benzoquinonato-κ2O,O′)ruthenium(II)