Crystal structure of 4,10-dimeth­oxy-13-methyl-6H,12H-6,12-epimino­dibenzob,f1,5dioxocine

Kasyanova K.V.; Kokozay V.N.; Buvaylo E.A.Vassilyeva O.Y.Skelton B.W.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Crystal structure of 4,10-dimethoxy-13-methyl-6H,12H-6,12-epiminodibenzob,f1,5dioxocine

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Crystal structure of 4,10-dimethoxy-13-methyl-6H,12H-6,12-epiminodibenzob,f1,5dioxocine

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The title compound, C17H17NO4, lacks crystallographic symmetry with one molecule per asymmetric unit. The molecule exists in a folded butterfly-like conformation; the benzene rings form a dihedral angle of 84.72 (7)°. The central eight-membered imino-bridged dioxocin ring adopts a twisted-boat conformation. In the crystal, inversion-related molecules are linked by pairs of weak C—H⋯O hydrogen bonds, forming double-stranded chains parallel to the a axis.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2017年第3期|410-412|共3页
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Kasyanova K.V.; Kokozay V.N.; Buvaylo E.A.Vassilyeva O.Y.Skelton B.W.;
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Crystal structure of 4,10-dimeth­oxy-13-methyl-6H,12H-6,12-epimino­dibenzob,f1,5dioxocine

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Crystal structure of 4,10-dimethoxy-13-methyl-6H,12H-6,12-epiminodibenzob,f1,5dioxocine