Crystal structure of 4-benzyl#173;carbamoyl-1-methyl#173;pyridin-1-ium iodide: an efficient multimodal anti#173;viral drug

Drebushchak T.N.; Kryukov Y.A.; Rogova A.I.Boldyreva E.V.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Crystal structure of 4-benzyl#173;carbamoyl-1-methyl#173;pyridin-1-ium iodide: an efficient multimodal anti#173;viral drug

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Crystal structure of 4-benzyl#173;carbamoyl-1-methyl#173;pyridin-1-ium iodide: an efficient multimodal anti#173;viral drug

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In the title compound, MeC5H4NCONHCH2C6H5I or C14H15N2O+#183;I#8722;, a cation and an anion form an ionic pair linked by a strong N#8212;H#8943;I hydrogen bond. In the crystal, ionic pairs linked by weak C#8212;H#8943;I hydrogen bonds form infinite ribbons along the crystallographic a axis. Polymorphism screening varying crystallization solvents (water, acetone 90#8211;water, ethanol 90#8211;water, 2-propanol 90#8211;water, DMF, DMSO, methanol, aceto#173;nitrile) and conditions (solution temperature, heating and cooling protocols) did not reveal any other polymorphs than the one reported in this work.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2017年第7期|967-970|共4页
作者
Drebushchak T.N.; Kryukov Y.A.; Rogova A.I.Boldyreva E.V.;
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作者单位

Institute of Solid State Chemistry and Mechanochemistry, SB RAS, ul. Kutateladze 18, Novosibirsk 630128, Russian Federation;

Novosibirsk State University, ul. Pirogova 2, Novosibirsk 630090, Russian Federation;

Institute for the Problems of the Technology of Energetic Materials, SB RAS, ul. Socialisticheskaia 1, Biisk 659322, Russian Federation;

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正文语种英语
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CRYSTAL STRUCTURE; DRUG; POLYMORPHISM;

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Crystal structure of 4-benzyl#173;carbamoyl-1-methyl#173;pyridin-1-ium iodide: an efficient multimodal anti#173;viral drug

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