Crystal structure of bis#173;2-(1H-benzimidazol-2-yl)anilinesilver(I) nitrate

Kim Y.; Kang S.K.

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Crystal structure of bis#173;2-(1H-benzimidazol-2-yl)anilinesilver(I) nitrate

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In the cation of the title salt, Ag(C13H11N3)2NO3, the AgI atom lies on a crystallographic inversion center and is coordinated by four N atoms from two bidentate 2-(1H-benzimidazol-2-yl)aniline ligands in a distorted square-planar geometry. The Ag#8212;N(aniline) bond 2.729#8197;(2)#8197;#197; is significantly longer than the Ag#8212;N(imidazole) bond 2.165#8197;(1)#8197;#197;. In the ligand, the aniline ring is twisted by 37.87#8197;(6)#176; from the mean plane of the benzimidazole ring system. The nitrate anion lies on a crystallographic twofold rotation axis which passes through the N atom and one of the O atoms. In the crystal, N#8212;H#8943;O hydrogen bonds link the components, forming a layer parallel to the bc plane.

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来源
《Acta Crystallographica Section E: Crystallographic Communications》 |2015年第9期|1058-1060|共3页
作者
Kim Y.; Kang S.K.;
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作者单位

Department of Chemistry, Chungnam National University, Daejeon 305-764, Republic of Korea;

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原文格式 PDF
正文语种英语
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CRYSTAL STRUCTURE; SILVER(I) COMPLEX; DISTORTED SQUARE-PLANAR GEOMETRY; BENZIMIDAZOLE; N-H...O HYDROGEN BONDS;

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2. Synthesis and Characterization of Silver(I) Nitrate Complexes with 2-, 3-, and 4- Cyano- Pyridines and Anilines [J] . I.S. Ahuja, Shailendra Tripathi, G.L. Yadava Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry . 1990,第2期

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Crystal structure of bis#173;2-(1H-benzimidazol-2-yl)anilinesilver(I) nitrate

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