Crystal structure of (4-fluoro#173;phenyl-#954;C1)iodido#173;(N,N,N#8242;,N#8242;-tetra#173;methyl#173;ethylenedi#173;amine-#954;2N,N#8242;)palladium(II)

Yan J.-J.; Zheng C.-G.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Crystal structure of (4-fluoro#173;phenyl-#954;C1)iodido#173;(N,N,N#8242;,N#8242;-tetra#173;methyl#173;ethylenedi#173;amine-#954;2N,N#8242;)palladium(II)

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Crystal structure of (4-fluoro#173;phenyl-#954;C1)iodido#173;(N,N,N#8242;,N#8242;-tetra#173;methyl#173;ethylenedi#173;amine-#954;2N,N#8242;)palladium(II)

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In the title compound, Pd(C6H4F)I(C6H16N2), the PdII atom is coordinated by two N atoms from the N,N,N#8242;,N#8242;-tetra#173;methyl#173;ethylenedi#173;amine ligand, a C atom of the 4-fluoro#173;phenyl group and an iodide ligand in a distorted square-planar geometry, with an average deviation from the least-squares plane through the ligand donor atoms of 0.0159#8197;(2)#8197;#197;. The angles about the PdII atom range from 83.35#8197;(16) to 178.59#8197;(11)#176;. In the crystal, weak C#8212;H#8943;F and C#8212;H#8943;I hydrogen bonds link the mol#173;ecules into sheets in the bc plane.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2015年第5期|共页
作者
Yan J.-J.; Zheng C.-G.;
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School of Chemical and Material Engineering, Jiangnan University, 1800 Lihu Road, Wuxi, Jiangsu Province 214122, People's Republic of China;

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CRYSTAL STRUCTURE; PALLADIUM(II) COMPLEX; TETRAMETHYLETHYLENEDIAMINE; SQUARE-PLANAR COORDINATION; SINGLE-CRYSTAL X-RAY STUDY; HYDROGEN BONDING;

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机译：四（6-甲基-2,2＆＃8242;-联吡啶）-1＆＃954; 2N，N＆＃8242 ;; 2＆＃954; 2N，N＆＃8242 ;; 3＆＃954; 2N，N＆＃8242 ;; 4＆＃954; 2N，N＆＃8242; -tetra-＆＃956; -nitrato-1：2＆＃954; 2O：O＆＃8242 ;; 2：3＆＃954; 3O：O＆＃8242 ;, O＆＃8242;＆＃8242 ;; 2：3＆＃954; 3O，O＆＃8242 ;: O＆＃8242;＆＃8242 ;; 3：4＆＃954; 2O：O＆＃8242; -tetranitrato-1＆＃954; 4O，O＆＃8242 ;; 4＆＃954; 2O，O＆＃8242; -tetralead（II）

Crystal structure of (4-fluoro#173;phenyl-#954;C1)iodido#173;(N,N,N#8242;,N#8242;-tetra#173;methyl#173;ethylenedi#173;amine-#954;2N,N#8242;)palladium(II)

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