Crystal structure of ethyl (2S)-9-meth#173;oxy-2-methyl-4-oxo-3,4,5,6-tetra#173;hydro-2H- 2,6-methano#173;benzog1,3,5oxa#173;diazocine-11-carboxyl#173;ate

Dhandapani A.; Manivarman S.; Subashchandrabose S.Gunasekaran B.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Crystal structure of ethyl (2S)-9-meth#173;oxy-2-methyl-4-oxo-3,4,5,6-tetra#173;hydro-2H- 2,6-methano#173;benzog1,3,5oxa#173;diazocine-11-carboxyl#173;ate

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Crystal structure of ethyl (2S)-9-meth#173;oxy-2-methyl-4-oxo-3,4,5,6-tetra#173;hydro-2H- 2,6-methano#173;benzog1,3,5oxa#173;diazocine-11-carboxyl#173;ate

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In the title compound, C15H18N2O5, the meth#173;oxy#173;phenyl ring makes a dihedral angle of 84.70#8197;(12)#176; with the mean plane of the tetra#173;hydro#173;pyrimidin-2(1H)-one ring. Both the pyran and tetra#173;hydro#173;pyrimidin-2(1H)-one rings have distorted envelope conformations with the carboxyl#173;ate-substituted C atom as the flap. In the crystal, mol#173;ecules are linked via pairs of N#8212;H#8943;O hydrogen bonds, forming zigzag chains propagating along 010, which enclose R22(8) ring motifs. The chains are linked by C#8212;H#8943;#960; inter#173;actions, forming a two-dimensional network parallel to (100).

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来源
《Acta Crystallographica Section E: Crystallographic Communications》 |2015年第2期|共页
作者
Dhandapani A.; Manivarman S.; Subashchandrabose S.Gunasekaran B.;
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作者单位

Post Graduate and Research Department of Chemistry, Government Arts College, C-Mutlur, Chidambaram 608 102, Tamil Nadu, India;

Centre for Research &

Development, PRIST University, Vallam, Thanjavur 613 403, Tamil Nadu, India;

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正文语种英语
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CRYSTAL STRUCTURE; HYDROPYRIMIDINE; OXADIAZOCINE; PYRAN; HYDROGEN BONDING;

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Crystal structure of ethyl (2S)-9-meth#173;oxy-2-methyl-4-oxo-3,4,5,6-tetra#173;hydro-2H- 2,6-methano#173;benzog1,3,5oxa#173;diazocine-11-carboxyl#173;ate

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