Crystal structure of cis-bis#173;(#956;-#946;-alanine-#954;2O:O#8242;)bistri#173;chlorido#173;rhenium(III)(Re#8211;Re) sesquihydrate

Golichenko A.A.; Domasevitch K.V.; Kytova D.E.Shtemenko A.V.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Crystal structure of cis-bis#173;(#956;-#946;-alanine-#954;2O:O#8242;)bistri#173;chlorido#173;rhenium(III)(Re#8211;Re) sesquihydrate

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Crystal structure of cis-bis#173;(#956;-#946;-alanine-#954;2O:O#8242;)bistri#173;chlorido#173;rhenium(III)(Re#8211;Re) sesquihydrate

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The structure of the title compound, Re2Cl6(C3H7NO2)2#183;1.5H2O, comprises a dinuclear complex cation Re#8212;Re = 2.2494#8197;(3)#8197;#197; involving cis-oriented double carboxyl#173;ate bridges, four equatorial chloride ions and two weakly bonded chloride ligands in the axial positions at the two rhenium(III) atoms. In the crystal, two complex mol#173;ecules and two water mol#173;ecules constitute hydrogen-bonded dimers, while an extensive hydrogen-bonding network involving the groups of the zwitterionic ligand is important for generation of the framework. An additional partially occupied water molecule is disordered over two sets of sites about a symmetry centre with a site-occupancy ratio of 0.3:0.2.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2015年第1期|45-47|共3页
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Golichenko A.A.; Domasevitch K.V.; Kytova D.E.Shtemenko A.V.;
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机译：Di - ＆＃956; 2-乙酸酯-1：2＆＃954; 2O：O＆＃8242 ;; 2：3＆＃954; 2O：O＆＃8242; -bis（N，N＆＃8242; - 二甲基甲酰胺）-1＆＃ 954; O，3＆＃954; O-bis {＆＃956; 2-2,2＆＃8242; - [丙烷-1,3-二基双（亚氨基亚甲基）]二酚盐-1＆＃954; 4O，N，N＆＃8242 ;，O＆＃8242;：2＆＃954; 2O，O＆＃8242 ;; 2＆＃954; 2O，O＆＃8242;：3＆＃954; 4O，N，N＆＃8242;，O＆＃8242; -1,3 -dinickel（II）-2-cadmium（II）

Crystal structure of cis-bis#173;(#956;-#946;-alanine-#954;2O:O#8242;)bistri#173;chlorido#173;rhenium(III)(Re#8211;Re) sesquihydrate

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