4-Bis(4-fluorophenyl)methylpiperazin-1-ium 2-(2-phenylethyl)benzoate

Betz R.; Dayananda A.S.; Gerber T.Hosten E.Yathirajan H.S.

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4-Bis(4-fluorophenyl)methylpiperazin-1-ium 2-(2-phenylethyl)benzoate

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The asymmetric unit of the title salt, C17H19F2N2+.C15H13O2−, derived from a 1,4-diazacyclohexane derivative and a carboxylic acid, contains two formula units. The cation is protonated at the secondary amine functionality. The six-membered heterocycles adopt chair conformations. The fluorophenyl rings in the two cations make dihedral angles of 77.21 (19) and 78.8 (2)° while the aromatic rings in the anions enclose angles of 69.5 (2) and 69.9 (2)°. In the crystal, classical N—H⋯O hydrogen bonds as well as C—H⋯F and C—H⋯O contacts connect the entities into layers parallel to ac.

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《Acta Crystallographica Section E: Crystallographic Communications》 |2011年第10期|o2783-o2784|共页
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Betz R.; Dayananda A.S.; Gerber T.Hosten E.Yathirajan H.S.;
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4-Bis(4-fluorophenyl)methylpiperazin-1-ium 2-(2-phenylethyl)benzoate

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