Ionothermal synthesis of novel Pb-OH-Cu-X (X = Cl, Br and I) quaternary heterometallic frameworks with tunable optical properties

Xue Ying-Ying; Zhang Li-Xia; Li Shu-NiJiang Yu-ChengHu Man-ChengZhai Quan-Guo

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Ionothermal synthesis of novel Pb-OH-Cu-X (X = Cl, Br and I) quaternary heterometallic frameworks with tunable optical properties

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Reported herein is the new application of ionothermal synthesis for inorganic optical materials. Under ionothermal conditions with different imidazolium ionic liquids, novel quaternary heterometallic frameworks based on Pb-4(OH)(4) cubane and CuCl4 or CuBr4 chains and Cu2I6 binuclear clusters have been successfully produced. Simple chlorine, bromine and iodine replacement leads to not only the space group change (tetragonal I41/acd for 1 and 2, and orthorhombic Fddd for 3) but also the topological net transformation (8,12-net for 1 and 2, and 6,6-net for 3). Notably, compounds 1, 2 and 3 all show tunable solid-state semiconducting and luminescence properties.

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《Dalton transactions: An international journal of inorganic chemistry》 |2017年第16期|5183-5188|共6页
作者
Xue Ying-Ying; Zhang Li-Xia; Li Shu-NiJiang Yu-ChengHu Man-ChengZhai Quan-Guo;
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Shaanxi Normal Univ, Sch Chem & Chem Engn, Key Lab Macromol Sci Shaanxi Prov, Xian 710062, Shaanxi, Peoples R China;

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正文语种英语
中图分类化学;无机化学;
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Ionothermal synthesis of novel Pb-OH-Cu-X (X = Cl, Br and I) quaternary heterometallic frameworks with tunable optical properties

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