Encapsulation of sodium alkyl sulfates by the cyclotriveratrylene-based, Pd6L812+ stella octangula cage?

Nikki J. Cookson; James J. Henkelis; Richard J. AnsellColin W. G. FishwickMichaele J. HardieJulie Fisher

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Encapsulation of sodium alkyl sulfates by the cyclotriveratrylene-based, Pd6L812+ stella octangula cage?

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We have previously described a cyclotriveratrylene (CTV)-based complex, Pd_6L_8~(12+), that forms a highly symmetric stella octangula cage. Here we report on the ability of this system to host sodium salts of three alkyl sulfates; octyl (SOS), dodecyl (SDS) and tetradecyl (STS). ~1H NMR chemical shift and diffusion coefficient measurements reveal that two molecules of alkyl sulfate reside in the cage, though rapid exchange between cage and bulk solvent is apparent. Host: guest association constants have been determined and support for the internalisation of the sulfates is available from 2D ROESY and NOESY data.

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《Dalton transactions: An international journal of inorganic chemistry》 |2014年第15期|5657-5661|共5页
作者
Nikki J. Cookson; James J. Henkelis; Richard J. AnsellColin W. G. FishwickMichaele J. HardieJulie Fisher;
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School of Chemistry, University of Leeds, Leeds, LS2 9JT, UK;

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正文语种英语
中图分类化学;无机化学;
关键词
SOS; SDS; NOESY;

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1. Encapsulation of sodium alkyl sulfates by the cyclotriveratrylene-based, [Pd6L8]12+ stella octangula cage? [J] . Nikki J. Cookson, James J. Henkelis, Richard J. Ansell, Dalton transactions: An international journal of inorganic chemistry . 2014,第15期

机译：[Pd6L8] 12+ Stella octangula笼中的烷基三硫酸钠对烷基硫酸钠的封装？
2. The interaction between sodium alkyl sulfate surfactants and the oppositely charged polyelectrolyte, polyDMDAAC, at the air-water interface: The role of alkyl chain length and electrolyte and comparison with theoretical predictions [J] . Penfold J, Tucker I, Thomas RKTaylor DJFZhang XLBell CBreward CHowell P Langmuir: The ACS Journal of Surfaces and Colloids . 2007,第6期

机译：The interaction between sodium alkyl sulfate surfactants and the oppositely charged polyelectrolyte, polyDMDAAC, at the air-water interface: The role of alkyl chain length and electrolyte and comparison with theoretical predictions
3. Effect of inorganic salt on adsorption of sodium alkyl sulfates and fatty acid sodium salts from aqueous solution onto ion exchange resins [J] . Yasuji Ihara journal of applied polymer science . 1988,第4期

机译：Effect of inorganic salt on adsorption of sodium alkyl sulfates and fatty acid sodium salts from aqueous solution onto ion exchange resins

Encapsulation of sodium alkyl sulfates by the cyclotriveratrylene-based, Pd6L812+ stella octangula cage?

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