Synthesis and characterization of LiMn2O4 powders by the combustion-assisted sol-gel technique

Wu XM.; Li XH.; Xiao ZB.Liu JB.Yan WB.Ma MY.

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Synthesis and characterization of LiMn2O4 powders by the combustion-assisted sol-gel technique

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LiMn2O4 powders were prepared by heating the ignited LiMn2O4 precursor gel using lithium acetate, manganese acetate, citric acid and glycol as starting materials. T e influence of synthesis conditions on the structural and electrochemical properties of LiMn2O4 was investigated by X-ray diffraction, scanning electron microscopy and charge-discharge experiments. The powders prepared under different conditions are of good crystallinity. The particle size, lattice parameter and the discharge capacity of LiMn2O4 powders increase with the increase of calcination temperature and calcination time. Except for the powder calcined at 750degreesC for I h, the powders prepared under other conditions show similar cycling behavior. (C) 2003 Elsevier B.V. All rights reserved. References: 14

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《Materials Chemistry and Physics》 |2004年第1期|182-186|共5页
作者
Wu XM.; Li XH.; Xiao ZB.Liu JB.Yan WB.Ma MY.;
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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种英语
中图分类工程材料学;
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Thermogravimetric analysis; Crystallisation; Electrochemical properties; Lithium manganese oxide; Citric-acid; Spinel; Batteries;

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Synthesis and characterization of LiMn2O4 powders by the combustion-assisted sol-gel technique

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