Solvothermal synthesis and phase control of nickel sulfides with different morphologies

Meng ZY.; Peng YY.; Yu WH.Qian YT.

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Solvothermal synthesis and phase control of nickel sulfides with different morphologies

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Nickel sulfides were prepared through a solvothermal process at 190degreesC by using NiCl2.6H(2)O and thiourea as reactants. XRD, XPS and SEM were used to study the phases, compositions and morphologies of the samples. it was found that through changing solvent and molar ratio of thiourea to NiCl2.6H(2)O, single-phase rhombohedral NiS (r-NiS) and hexagonal NiS (h-NiS) were obtained, NiS2 and Ni3S4 were also observed. r-NiS prepared in different solvents had different morphologies, such as rod-, sphere-, and petal-like. (C) 2002 Elsevier Science B.V. All rights reserved. References: 17

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《Materials Chemistry and Physics》 |2002年第2期|230-233|共4页
作者
Meng ZY.; Peng YY.; Yu WH.Qian YT.;
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作者单位

Project Leader,Animal Health and Welfare,Cheshire County Council;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种英语
中图分类工程材料学;工程基础科学;
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机译：Phase-controlled solvothermal syntheses and oxygen evolution reaction (OER) activity of nickel sulfide nanoparticles obtained from 1,2-bis(diphenylphosphino)ethane nickel() acetylacetonatedithiolate
2. Solvent-free synthesis of morphology-controllable nickel sulfides via one-pot plasma reactions for high-performance lithium-ion batteries [J] . Yang Yinghui, Wang Junzhang, Wang ChaoGuan RongzhangLu DujiangZhao ShuchunLiu ShuaiBian Xiufang Green chemistry . 2020,第21期

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3. Thermodynamic-controlled gas phase process for the synthesis of nickel nanoparticles of adjustable size and morphology [J] . Kauffeldt E, Kauffeldt T Journal of nanoparticle research: An interdisciplinary forum for nanoscale science and technology . 2006,第4期

机译：Thermodynamic-controlled gas phase process for the synthesis of nickel nanoparticles of adjustable size and morphology
4. Systematic morphology and phase control of Mg-ptcda coordination polymers by Ostwald ripening and self-templating [O] . Zhao Jiao, Su Panpan, Zhao Yaopeng, 2012

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5. Synthesis, characterization and reactivity of high oxidation state nickel fluorides [R] . Chacon, L. C. 1997

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Solvothermal synthesis and phase control of nickel sulfides with different morphologies

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