The crystallisation of copper(II) phenylphosphonates

Wilke Manuel; Kabelitz Anke; Gorelik Tatiana E.Buzanich Ana GuilhermeReinholz UweKolb UteRademann KlausEmmerling Franziska

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The crystallisation of copper(II) phenylphosphonates

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The crystal structures and syntheses of four different copper(II) phenylphosphonates, the monophenyl-phosphonates alpha-, beta-, and gamma-Cu(O3PC6H5)center dot H2O (alpha-CuPhPmH (1) beta-CuPhPmH (2) and gamma-CuPhPmH (3)), and the diphosphonate Cu(HO3PC6H5)(2)center dot H2O (CuPhP2mH (4)), are presented. The compounds were synthesized from solution at room temperature, at elevated temperature, under hydrothermal conditions, and mechanochemical conditions. The structures of alpha-CuPhPmH (1) and CuPhP2mH (4) were solved from powder X-ray diffraction data. The structure of beta-CuPhPmH (2) was solved by single crystal X-ray analysis. The structures were validated by extended X-ray absorption fine structure (EXAFS) and DTA analyses. Disorder of the crystal structure was elucidated by electron diffraction. The relationship between the compounds and their reaction pathways were investigated by in situ synchrotron measurements.

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《Dalton transactions: An international journal of inorganic chemistry》 |2016年第43期|17453-17463|共11页
作者
Wilke Manuel; Kabelitz Anke; Gorelik Tatiana E.Buzanich Ana GuilhermeReinholz UweKolb UteRademann KlausEmmerling Franziska;
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BAM Fed Inst Mat Res & Testing, Richard Willstatter Str 11, D-12489 Berlin, Germany;

Johannes Gutenberg Univ Mainz, Inst Phys Chem, Welderweg 11, D-55128 Mainz, Germany;

Humboldt Univ, Dept Chem, Brook Taylor Str 2, D-12489 Berlin, Germany;

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正文语种英语
中图分类化学;无机化学;
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The crystallisation of copper(II) phenylphosphonates

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