Crystal growth and characterization of 4-nitro-4 '-methoxy benzylidene aniline (NMOBA)

Azariah  AN; Hameed  ASH; Thenappan  TNoel  MRavi  G

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Crystal growth and characterization of 4-nitro-4 '-methoxy benzylidene aniline (NMOBA)

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We report the crystal growth studies of 4-nitro-4'-methoxy benzylidene aniline (NMOBA). NMOBA was synthesized by the condensation of the corresponding aniline and aldehyde. Formation of the product was confirmed from the FTIR and NMR spectral analyses. Powder second harmonic generation analysis of the crystal showed that its efficiency is 1.24 times than that of KDP. The solubility of NMOBA was determined in toluene at different temperatures. Single crystals were grown from toluene by restricted evaporation and slow cooling methods. The structural characterization of the grown crystal was carried out by X-ray diffraction method and the thermal properties were studied by TGA, DTA and DSC experiments and optical transparency of the sample was determined by UV-VIS-NIR spectroscopy. (C) 2004 Elsevier B.V. All rights reserved.

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《Materials Chemistry and Physics》 |2004年第1期|90-96|共7页
作者
Azariah AN; Hameed ASH; Thenappan TNoel MRavi G;
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作者单位

Alagappa Univ, Crystal Res Ctr, Karaikkudi 630003, Tamil Nadu, India;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种英语
中图分类工程材料学;
关键词
organic crystals; benzylidene aniline; solution growth; XRD data; NONLINEAR-OPTICAL-MATERIALS; ORGANIC-SOLVENTS;

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Crystal growth and characterization of 4-nitro-4 '-methoxy benzylidene aniline (NMOBA)

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