A nonanuclear triangular macrocycle and a linear heptanuclear heterometallic complex based on a 2-substituted imidazole-4,5-dicarboxylate ligand

Lin Yue-Jian; Shan Wei-Long; Jin Guo-Xin

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A nonanuclear triangular macrocycle and a linear heptanuclear heterometallic complex based on a 2-substituted imidazole-4,5-dicarboxylate ligand

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摘要

A (CpRh)-Rh-star-based nonanuclear triangular macrocycle complex ((CpRh)-Rh-star)(9)L-3(NO3)(4.5)(MeOH)(OTf)(4.5) (1), a (CpIr)-Ir-star-based trinuclear complex ((CpIr)-Ir-star)(3)L(MeCN)(4)(OTf)(3) (2) and a linear heptanuclear heterometallic complex ((CpIr)-Ir-star)(6)ZnL2(MeCN)(8)(MeOH)(2)(OTf)(8) (3) (Cp-star = eta(5)-pentamethylcyclopentadienyl) have been synthesized from a 2-(4-(pyridin-4-yl)phenyl)-1H-imidazole-4,5-dicarboxylic acid proligand. These complexes were further characterized by X-ray crystallography, H-1 NMR, DOSY NMR, IR spectroscopy, and elemental analyses.

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《Dalton transactions: An international journal of inorganic chemistry》 |2016年第32期|12680-12684|共5页
作者
Lin Yue-Jian; Shan Wei-Long; Jin Guo-Xin;
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作者单位

Fudan Univ, Dept Chem, Collaborat Innovat Ctr Chem Energy Mat, State Key Lab Mol Engn Polymers, Shanghai 200433, Peoples R China;

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正文语种英语
中图分类化学;无机化学;
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A nonanuclear triangular macrocycle and a linear heptanuclear heterometallic complex based on a 2-substituted imidazole-4,5-dicarboxylate ligand

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