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Analysis of Adhesion Test Methods and the Evaluation of Their Use for Ion-Beam-Mixed Metal/Ceramic Systems

机译:离子束混合金属/陶瓷体系粘附性试验方法分析及其用途评价

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Several thin film adhesion tests have been examined to determine which provides the most reliable method for the measurement of the adhesion of thin metallic films to ceramic substrate. An attempt was made to use the testing techniques described to measure adhesion changes caused by ion beam mixing for a variety of metal/ceramic systems. The techniques analyzed were the scratch test, the acoustic-emission test, and the pull test. The major variables of the scratch test include film thickness, substrate hardness, and stylus radius, but it is not known precisely what effects changes in these have on the measurement of adhesion. The scratch analyses methods discussed in the literature, each describing a load or stress on the system that is presumed to cause de-adhesion, do not always hold because none of the analyses account for both plastic and elastic deformation or incorporate many of the important parameters. The scratch test was much more likely to reveal a critical value for de-adhesion for relatively brittle films such as chromium than for ductile films such as nickel. 65 refs, 29 figs, 17 tabs. (ERA citation 13:051611)

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