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Determination of Beryllium in Urine,Hair, Fingernail,and Fecal Samples by Flameless Atomic Absorption Spectrometry.

机译:无火焰原子吸收光谱法测定尿液,头发,指甲和粪便样品中的铍。

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Methods for determining trace amounts of beryllium in urine,hair,fingernail,and fecal samples are described. These methods involve use of a Perkin-Elmer Model 503spectrophotometer equipped with an HGA-2100graphite furnace. Lanthanum was used as a masking and enhancing agent,and recoveries were determined by direct comparison with aqueous standards. The hair and fingernail samples were degraded readily in a nitric acid-perchloric acid mixture,and the feces were digested rapidly using a ferrous ion,hydrogen peroxide method. The urine samples were run by two methods: (1) direct and (2) coprecipitation. Nanogram-per-gram levels of beryllium were recovered from all tissues and fluids. All recoveries varied from 90to 110percent with relative standard deviations of less than 13percent. (ERA citation 01:024046)

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