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Capillary Column GC-MS Determination of 77 Purgeable Organic Compounds in Two Simulated Liquid Wastes

机译：毛细管柱GC-ms测定两种模拟液体废物中77种可清除的有机化合物

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The suitability of purge-trap-desorb (PTD) procedures for determination of 84 volatile organic compounds with capillary column gas chromatograph (GC) and mass spectrometry (MS) was evaluated. After collecting GC-MS data not previously available for some analytes, 7 of the 84 compounds were eliminated from further consideration because of poor purging efficiency or analyte instability. For each of the remaining 77 compounds, the linear concentration range and detection limit were determined with data obtained by PTD GC-MS analysis of spiked reagent water. The criterion was met over a concentration range of at least two orders of magnitude for 56 of the 77 analytes, 1.5 orders of magnitude for 12 analytes, and 1 order of magnitude for 6 analytes. The criterion was not met for acetone, trichlorofluoromethane, and 2-chloro-1,3-butadiene. Method performance was assessed by analyzing eight replicate aliquots of two simulated liquid waste samples (a municipal sewage sludge leachate and water containing fulvic acid) containing analytes spiked at two concentrations.

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Yancey, M. F. ; Kornfeld, R. A. ; Warner, J. S.;
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年度 1988
页码 1-80
总页数 80
原文格式 PDF
正文语种 eng
中图分类工业技术;
关键词
Water pollution detection; Gas chromatography; Mass spectroscopy; Concentration(Composition); Environmental monitoring; Determination; Samples; Simulation; Effluents; Water quality; Standard deviation;

机译：水污染检测;气相色谱;质谱;浓度（成分）;环境监测;测定;样品;模拟;废水;水质;标准偏差;

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专利

1. Critical comparison of automated purge and trap and solid-phase microextraction for routine determination of volatile organic compounds in drinking waters by GC-MS [J] . Lara-Gonzalo A, Sanchez-Uria JE, Segovia-Garcia E, Talanta: The International Journal of Pure and Applied Analytical Chemistry . 2008,第5期

机译：全自动吹扫捕集和固相微萃取用于GC-MS常规测定饮用水中挥发性有机化合物的关键比较
2. PURGE AND TRAP EXTRACTION WITH GC-MS DETERMINATION OF VOLATILE ORGANIC COMPOUNDS IN TABLE-READY FOODS [J] . Heikes DL, Jensen SR, Flemingjones ME Journal of Agricultural and Food Chemistry . 1995,第11期

机译：气相色谱-质谱法测定台式食品中的挥发性有机化合物的吹扫和捕集
3. Separation and Identification of Volatile Compounds from Liquid Cultures of Trichoderma harzianum by GC-MS using Three Different Capillary Columns [J] . Shafiquzzaman Siddiquee, Bo Eng Cheong, Khanam Taslima, Journal of Chromatographic Science . 2012,第4期

机译：使用三种不同的毛细管柱，通过GC-MS从哈茨木霉液体培养物中分离和鉴定挥发性化合物
4. Determination of 5 odorous compounds in water by GC-MS/MS using purge-and-trap technique [C] . Xiaohua Liu, Ying Ye, Ning Yuan, ASMS Conference on Mass Spectrometry and Allied Topics . 2015

机译：使用吹扫和捕获技术测定GC-MS / MS水中的5种异血化合物
5. DETERMINATION OF POLYCYCLIC AROMATIC COMPOUNDS BY CAPILLARY GAS CHROMATOGRAPHY - MASS SPECTROMETRY: STUDIES OF BIOCONCENTRATION IN VERTEBRATE FISH (GC-MS). [D] . VASSILAROS, DANIEL L. 1983

机译：毛细管气相色谱-质谱法测定多环芳族化合物：无脊椎动物鱼中生物富集度的研究（GC-MS）。
6. Multidimensional Liquid Chromatography Employing a Graphene Oxide Capillary Column as the First Dimension: Determination of Antidepressant and Antiepileptic Drugs in Urine [O] . Edvaldo Vasconcelos Soares Maciel, Ana Lúcia de Toffoli, Jussara da Silva Alves, 2020

机译：以氧化石墨烯毛细管柱为一维的多维液相色谱法：尿液中抗抑郁药和抗癫痫药的测定
7. Separation and Identification of Volatile Compounds from Liquid Cultures of Trichoderma harzianum by GC-MS using Three Different Capillary Columns [O] . S. Siddiquee, B. E. Cheong, K. Taslima, 2012

机译：用三种不同毛细管通过GC-MS从吡氏霉菌液体培养物中挥发性化合物的分离和鉴定
8. Capillary Column GC-MS Determination of 77 Purgeable Organic Compounds in Two Simulated Liquid Wastes. Project Summary. [R] . Yancey, M. F., Kornfeld, R. A., Warner, J. S. 1988

机译：毛细管柱GC-ms测定两种模拟液体废物中77种可清除的有机化合物。项目总结。

Capillary Column GC-MS Determination of 77 Purgeable Organic Compounds in Two Simulated Liquid Wastes

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