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Trenbolone Acetate and Trenbolone: Trace Analysis in Animal Chow, Wastewater and Human Urine by High Pressure Liquid Chromatography and Electron Capture Gas Chromatography

机译：Trenbolone acetate和Trenbolone：高压液相色谱和电子捕获气相色谱法测定动物饲料，废水和人尿中的痕量

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Only a few procedures for determining TBA and TBOH have appeared in the literature. Thin layer chromatography (TLC) has been used to separate TBA from TBOH. Radioimmunoassay (RIA) procedures for the compounds in bovine tissue and plasma have been described and used to determine residues of TBA in tissues from calves treated with TBA and estradiol. The TLC procedure apparently lacks the precision required for assays of the dosage form and RIA capability has not been developed in the author's laboratory. Therefore, a method was devised for assaying traces of both compounds in animal chow via high pressure liquid chromatography (HPLC). Also, both compounds were found to react with pentafluorophropionic anhydride to form the corresponding pentafluoropropionyl IPFP) derivatives, which were analyzed by electron-capture gas chromatography (EC/GC). These procedures were subsequently modified for the analysis of human urine and waste water.

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作者
Holder, C. L.;
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年度 1979
页码 1-28
总页数 28
原文格式 PDF
正文语种 eng
中图分类工业技术;
关键词
Toxicology; Chemical analysis; Bioassay; Trace elements; Environmental surveys; Dosage; Residues; Tissues(Biology); Gas chromatography; Water analysis; Urine; Chromatographic analysis; Laboratory animals; Thin layer chromatography; Waste disposal;

机译：毒理学;化学分析;生物测定;微量元素;环境调查;剂量;残留;组织（生物学）;气相色谱;水分析;尿液;色谱分析;实验动物;薄层色谱;废物处理;
入库时间 2022-08-29 11:27:03

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机译：电子捕获气相色谱法用于芳烃分析。关于在有机分析中使用电子捕获气相色谱的协调计划的一部分。 1977年4月1日期间的最终报告

Trenbolone Acetate and Trenbolone: Trace Analysis in Animal Chow, Wastewater and Human Urine by High Pressure Liquid Chromatography and Electron Capture Gas Chromatography

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