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A One Step Method for the Determination of Carbamate Pesticides by Derivatization with alpha-Bromo-2,3,4,5,6-Pentafluorotoluene

机译：用α-溴-2,3,4,5,6-五氟甲苯衍生化测定氨基甲酸酯类农药的一步法

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摘要

A procedure was developed for the determination of trace quantities of a broad range of carbamate pesticides. The carbamates were hydrolyzed and derivatized in a single step, using alkali and alpha-bromo-2,3,4,5,6-pentafluorotoluene (PFBB), and were subsequently analyzed using electron capture gas chromatography. This one step derivatization method created a novel derivative in which one fluorine on the PFB ring was displaced by an ethoxide ion via aromatic nucleophilic substitution.

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Jackson, M. D. ; Soileau, S. D. ; Sovocool, G. W. ; Sachleben, R. A.;
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年度 1979
页码 1-106
总页数 106
原文格式 PDF
正文语种 eng
中图分类工业技术;
关键词
Pesticides; Carbamates; Chemical analysis; Trace elements; Hydrolysis; Bromine organic compounds; Gas chromatography;

机译：农药;氨基甲酸酯;化学分析;微量元素;水解;溴有机化合物;气相色谱法;

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1. Trace level determinations of carbamate pesticides in surface water by gas chromatography-mass spectrometry after derivatization with 9-xanthydrol [J] . Yang E.-Y., Shin H.-S. Journal of chromatography, A: Including electrophoresis and other separation methods . 2013,第Null期

机译：9-Xanthydrol衍生化后气相色谱-质谱法测定地表水中的氨基甲酸酯类农药
2. Low-density solvent based ultrasound-assisted emulsification microextraction and on-column derivatization combined with gas chromatography-mass spectrometry for the determination of carbamate pesticides in environmental water samples [J] . Guo L., Lee H.K. Journal of chromatography, A: Including electrophoresis and other separation methods . 2012,第Null期

机译：低密度溶剂超声辅助乳化微萃取-柱上衍生-气相色谱-质谱联用测定环境水样中的氨基甲酸酯类农药
3. Determination of Four Carbamate Pesticides in Corn by Cloud Point Extraction and High-Performance Liquid Chromatography in the Visible Region Based on Their Derivatization Reaction [J] . Zhi-ming Zhou, Jian-bo Chen, Dao-yuan Zhao Journal of Agricultural and Food Chemistry . 2009,第19期

机译：基于衍生化反应的可见点浊点萃取-高效液相色谱法测定玉米中四种氨基甲酸酯类农药
4. Sensitive and Selective LC/MS/MS Method for Determination of Endogenous Cholestane-3beta,5alpha,6beta-triol in Human Plasma after Derivatization with N,N-Dimethylglycine [C] . Xuntian Jiang, Hideji Fujiwara, Rohini Sidhu, American Society for Mass Spectrometry Conference on Mass Spectrometry and Allied Topics . 2010

机译：衍生化与N，N-二甲基甘氨酸衍生后，敏感和选择性LC / MS / MS / MS / MS / MS / MS / MS法测定人血浆中的人血浆中的5Alpha，6beta-Trin
5. INVESTIGATION OF METAL HYDRIDES USING MULTIPLE WAVELENGTH NEUTRON POWDER DIFFRACTION AND THE CRYSTAL STRUCTURE DETERMINATIONS OF THE 2,4-DINITROPHENYLHYDRAZONE DERIVATIVE OF 5-BROMOMETHYLIDENE CYCLONONANONEAND THE 1-HYDROXY-6-ACETOXY- 10 ALPHA- BROMO-BICY [D] . DEHAVEN, PATRICK WILLIAM. 1977

机译：多波长中子粉末衍射法研究金属氢化物以及5-溴代乙炔环酮和1-羟基-6-环己酮-10-羟基10的2，4-二苯并吡嗪酮衍生物的晶体结构测定
6. Simultaneous Determination of Glutamate Glycine and Alanine in Human Plasma Using Precolumn Derivatization with 6-Aminoquinolyl-N-hydroxysuccinimidyl Carbamate and High-Performance Liquid Chromatography [O] . Qing Zhong Li, Qing Xian Huang, Shu Cui Li, 2012

机译：使用6-氨基喹啉基-N-羟基琥珀酰亚胺氨基甲酸酯的柱前衍生化和高效液相色谱法同时测定人血浆中的谷氨酸甘氨酸和丙氨酸
7. Application of a Micro Multiphase Laminar Flow on a Microchip for Extraction and Determination of Derivatized Carbamate Pesticides [O] . Adelina SMIRNOVA, Kiyohito SHIMURA, Akihide HIBARA, 2007

机译：微相杂交流动对微芯片萃取和测定衍生氨基甲酸杀虫剂的应用
8. A One-Step Derivatization Procedure for Several Carbamate Pesticides [R] . Jackson, M. D. , Soileau, S. D. 1981

机译：几种氨基甲酸酯类农药的一步衍生化方法

A One Step Method for the Determination of Carbamate Pesticides by Derivatization with alpha-Bromo-2,3,4,5,6-Pentafluorotoluene

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