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Annealing and Precipitation Behavior During Batch Annealing of HSLA Steels

机译:HSLA钢分批退火过程中的退火和析出行为

摘要

To gain a fundamental understanding of the factors responsible for the kinetics of annealing behavior during batch annealing for high strength low alloy (HSLA) steels, studies have been conducted to analyze the influence of alloy composition, hot band state, cold rolling reduction (CR%), heating rate, soaking temperature and time, etc. on the annealing behavior of HSLA steels during batch annealing process. The recrystallization kinetics was mainly controlled by several key parameters such as stored energy, precipitation and/or solute drag, special grain boundaries, and texture, etc. The combination of Electron Back-Scattered Diffraction (EBSD) technique and the Sub-grain Method was used to construct and analyze stored energy distribution maps before and during the batch annealing process of cold rolled HSLA steels. Precipitation behavior was studied using Scanning Electron Microscopy (SEM), Energy Dispersive X-ray Spectroscopy (EDS), Transmission Electron Microscopy (TEM), and High Resolution TEM (TEM). Grain boundary characteristic and texture fibers were also analyzed using EBSD scanning data. The results show that different composition and processing parameters would cause different hot band microstructure and different amounts of dislocation density, i.e., stored energy, remained in the alloys after hot rolling deformation. Higher dislocation density in the hot band steel will cause even higher dislocation density in the sheet steel after cold rolling deformation, which will cause higher recrystallization speed at early stages. If precipitates were formed during annealing, their formation would consume part of the stored energy and decreased some driving force. The new formed fine TiC precipitates would also apply certain pinning force on the grain boundaries, which dragged the moving of those boundaries, i.e., lowered the recrystallization speed further. Certain special grain boundaries like Coincident Site Lattice (CSL) boundaries have very low boundary energy and mobility. The higher volume fraction of this kind of boundaries would also slow down the recrystallization process. Texture could not be a critical factor causing the different annealing behavior in this study, since the texture fibers distributions are very similar. Two or more factors might affect the annealing process at the same time. Some factors could be more efficient than others at certain stage or stages.
机译:为了对高强度低合金(HSLA)钢的批量退火过程中引起退火行为动力学的因素有基本的了解,已经进行了研究以分析合金成分,热带状态,冷轧压下率(CR%)的影响。 ),加热速率,均热温度和时间等因素对HSLA钢分批退火过程中退火行为的影响。再结晶动力学主要受几个关键参数控制,例如储能,沉淀和/或溶质阻力,特殊的晶界和织构等。电子背散射衍射(EBSD)技术与亚晶粒方法的结合是用于在冷轧HSLA钢的批量退火之前和期间构造和分析存储的能量分布图。使用扫描电子显微镜(SEM),能量色散X射线光谱仪(EDS),透射电子显微镜(TEM)和高分辨率TEM(TEM)研究了沉淀行为。还使用EBSD扫描数据分析了晶界特征和纹理纤维。结果表明,在热轧变形后,不同的组成和加工参数将导致不同的热带显微组织和不同数量的位错密度,即储存的能量。热轧带钢中较高的位错密度将导致冷轧变形后钢板中的较高位错密度,这将导致早期的较高再结晶速度。如果在退火期间形成沉淀物,则沉淀物的形成将消耗一部分存储的能量并降低一些驱动力。新形成的细小的TiC沉淀也会在晶界上施加一定的钉扎力,这会拖延那些晶界的移动,即,进一步降低了再结晶速度。某些特殊的晶界,例如重合点晶格(CSL)边界,其边界能和迁移率非常低。这种边界的较高体积分数也会减慢重结晶过程。由于纹理纤维的分布非常相似,因此纹理在本研究中不是导致不同退火行为的关键因素。两个或多个因素可能同时影响退火过程。在某些阶段或某些阶段,某些因素可能比其他因素更有效率。

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  • 作者

    Fang Chao;

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  • 年度 2011
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  • 原文格式 PDF
  • 正文语种 {"code":"en","name":"English","id":9}
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