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Full-field method for statistical evaluation and characterization of the fluid-induced stress in the micro-range for microstructures of alloys

机译:用于合金微观结构微观范围内流体诱导应力统计评估和表征的全场方法

摘要

Statistical and characterizing full-field method of fluid stress in the micro-range for microstructures of alloys, which comprises the following steps: a) The grinding and polishing of the surface of an alloy sample to a high-gloss finish without grinding errors and then the definition of an area to be measured on the surface of the alloy sample; the size of the area to be measured being 1 - 25 mm × 1 - 25 mm; b) the use of a white light interferometric 3D surface profilometer to measure the initial morphology on the surface of the alloy sample in order to determine the size, obtain the spacing and length-to-width ratio of microstructures on the starting surface of the alloy; c) using isostatic pressing technology to obtain the microstructural deformation on the surface of the alloy sample, and then using a white light 3D interferometric surface profilometer to measure the deformed morphology on the surface of the alloy sample to obtain the size, spacing and length to width ratio of the deformed microstructures on the surface of the alloy; to perform the statistical analysis based on the comparison between the size, the distances and the ratio of length to width of the microstructures on the surface of the alloy and those on the deformed microstructures on the surface of the alloy to obtain the deformation data on the surface of the alloy to obtain; and the mapping to obtain the deformation resistance of the microstructures on the surface of the alloy; and the associated calculations to obtain a spectrum of changes in micromorphology in terms of size, spacing and length to width ratio of the microstructures on the surface of the alloy based on the distribution of resistance to deformation of the microstructures on the surface of the alloy; d ) performing the oversized and rapid characterization of the quantitative statistical distribution of the morphological changes before and after isostatic pressing of the microstructures in the area of the alloy to be measured, so that a corresponding full-field metallographic spectrum is obtained.
机译:统计和表征合金微观结构微观范围内流体应力的全场方法,包括以下步骤:a)将合金样品的表面打磨和抛光至高光泽度而没有打磨误差,然后合金样品表面上待测量区域的定义;被测区域的尺寸为1-25 mm×1-25 mm; b)使用白光干涉3D表面轮廓仪测量合金样品表面的初始形态,以确定尺寸,获得合金起始表面上微观结构的间距和长宽比; c)使用等静压技术获得合金样品表面的微观结构变形,然后使用白光3D干涉表面轮廓仪测量合金样品表面的变形形态,以获得尺寸,间距和长度合金表面变形后的微观结构的宽度比;根据合金表面微观组织的尺寸,距离和长宽比与变形后的微观组织的尺寸,距离和长宽比之间的比较,进行统计分析,以得到合金表面的变形数据。获得合金表面;并绘制以获得合金表面上的微结构的抗变形性;以及相关的计算,以基于合金表面上微结构变形抗力的分布,得出微观形貌在尺寸,间距和长度上的宽度比方面的变化光谱; d)在待测合金区域中对组织进行等静压之前和之后,对形态变化的定量统计分布进行超大尺寸和快速的表征,从而获得相应的全场金相光谱。

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