首页> 外国专利> METHOD OF PREPARING SAMPLES OF OIL-FIELD CHEMICALS FOR DETERMINING ORGANOCHLORINE COMPOUNDS AND ORGANICALLY BOUND CHLORINE

METHOD OF PREPARING SAMPLES OF OIL-FIELD CHEMICALS FOR DETERMINING ORGANOCHLORINE COMPOUNDS AND ORGANICALLY BOUND CHLORINE

机译:制备用于测定有机氯化合物和有机结合氯的油类化学品样品的方法

摘要

FIELD: chemistry.;SUBSTANCE: invention relates to analytical chemistry and specifically to a method for preparing samples of oil-field reagents. Method of preparing samples of oil-field chemicals for determining organochlorine compounds and organically bound chlorine involves separating salts of quaternary ammonium compounds to eliminate the effect of products of their thermal decomposition, wherein analyzed sample, polar and non-polar solvents are extracted in equal proportions, extraction of mixture with transition of quaternary ammonium compounds to polar phase, and organochlorine compounds in a nonpolar phase with subsequent extraction of an aliquot of an extract of a nonpolar solvent for analysis.;EFFECT: high accuracy and reliability of determining quantitative content of organochlorine compounds present in reagents.;5 cl, 7 dwg, 1 tbl
机译:油田试剂的制备方法技术领域本发明涉及分析化学,尤其涉及一种油田试剂的制备方法。制备用于测定有机氯化合物和有机结合氯的油田化学品样品的方法涉及分离季铵化合物的盐以消除其热分解产物的影响,其中分析样品,极性和非极性溶剂按等比例提取,在季铵化合物转变为极性相的混合物中进行萃取,在非极性相中萃取有机氯化合物,随后萃取非极性溶剂萃取物等分试样进行分析的方法;效果:测定有机氯定量含量的准确性和可靠性试剂中存在的化合物; 5 cl,7 dwg,1 tbl

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