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Manufacturing method of lanthanum zirconate powder for thermal barrier coatings
Manufacturing method of lanthanum zirconate powder for thermal barrier coatings
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机译:用于热障涂层的锆酸镧粉末的制造方法
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摘要
In the present invention, lanthanum nitrate hydrate (La(NO 3 ) 3 · nH 2 O, x is a natural number of 10 or less) powder, yttrium nitrate hydrate (Y(NO 3 ) 3 ·nH 2 O, x is 10 or less Natural water) mixing the powder and zirconyl chloride hydrate (ZrOCl 2 ·nH 2 O, x is a natural water of 10 or less) in a solvent to form a mixture, mixing the mixture with oxalic acid, and the mixture and the Adding a mixed solution of oxalic acid to the basic solution to form a precipitate, filtering and drying the precipitate, and calcining the dried product (La 1-x Y x ) 2 Zr 2 O 7 (0 x 1) relates to a method for producing a lanthanum zirconate-based powder for thermal barrier coating comprising the step of obtaining a powder. The lanthanum zirconate-based powder for thermal barrier coating produced by the present invention has low thermal conductivity, high chemical resistance and corrosion resistance, and is utilized as a thermal barrier coating material for gas turbine engines or internal combustion engines used at high temperatures. Can be.
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机译:在本发明中,硝酸镧水合物(La(NO 3 Sub>) 3 Sub>·nH 2 Sub> O,x为10以下的自然数。 )粉末,硝酸钇水合物(Y(NO 3 Sub>) 3 Sub>·nH 2 Sub> O,x为10或更少的天然水)混合粉末和溶剂中的水合氧化锆(ZrOCl 2 Sub>·nH 2 Sub> O,x为10以下的天然水)形成混合物,将混合物与草酸混合,然后将混合物和草酸的混合溶液添加到碱性溶液中形成沉淀,过滤并干燥沉淀,然后煅烧干燥后的产物(La 1 Sub> - Sub > x Sub> Y x Sub>) 2 Sub> Zr 2 Sub> O 7 Sub>(0 展开▼