首页> 外国专利> QUALITATIVE AND QUANTITATIVE ANALYSIS METHOD OF SOLID ELECTOLYTE INTERPHASE FILM OF A SECONDARY BATTERY

QUALITATIVE AND QUANTITATIVE ANALYSIS METHOD OF SOLID ELECTOLYTE INTERPHASE FILM OF A SECONDARY BATTERY

机译:二次电池固体电解质相膜的定性定量分析方法

摘要

The present invention provides a quantitative and qualitative analysis method for an electrode film for a secondary battery, which comprises the steps of: accommodating an electrode assembly including an anode, a cathode, and a separator in a battery case; preparing a preliminary lithium secondary battery by injecting a non-aqueous electrolyte solution containing a lithium salt, an organic solvent, and an additive for forming a solid electrolyte interface (SEI) film into the battery case; forming the preliminary lithium secondary battery; decomposing the preliminary lithium secondary battery to obtain at least one electrode of the anode and the cathode; washing the obtained electrode; dipping the washed electrode in an extraction solvent to extract an SEI film on an electrode surface; and analyzing inorganic components in the extraction solvent by using capillary electrophoresis. Therefore, the inorganic components of the SEI film formed on the electrode surface can be analyzed qualitatively and quantitatively.
机译:本发明提供了用于二次电池的电极膜的定量和定性分析方法,其包括以下步骤:将包括阳极,阴极和隔板的电极组件容纳在电池盒中;通过将包含锂盐,有机溶剂和用于形成固体电解质界面(SEI)膜的添加剂的非水电解质溶液注入到电池盒中来制备预备锂二次电池;形成预备锂二次电池;分解预备锂二次电池以获得阳极和阴极中的至少一个电极;洗涤获得的电极;将洗涤后的电极浸入提取溶剂中,以在电极表面上提取SEI膜;毛细管电泳法分析萃取溶剂中的无机成分。因此,可以定性和定量地分析在电极表面上形成的SEI膜的无机成分。

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