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DEVICE AND METHOD FOR SIMULTANEOUSLY DETERMINING TEMPERATURE-DEPENDENT THERMAL CONDUCTIVITY, THERMAL DIFFUSIVITY AND SPECIFIC HEAT CAPACITY

机译:同时确定与温度有关的热导率,热扩散率和比热容的装置和方法

摘要

The invention relates to a device and a method for simultaneously determining temperature-dependent thermal conductivity, thermal diffusivity and specific heat capacity and comprises a heat source for locally heating a solid body to be examined, a both locally and chronologically high-resolution line and/or surface detector for non-contact temperature measurement along the sample, and a cooling circuit having a cooling liquid flowing around the lower sample edge, the temperature increase and flow rate of which cooling liquid are measured continuously. The thermal diffusivity is determined by means of the described method from the transient thermal states of the sample, which are adjusted in a controlled manner, during heating and cooling. The thermal conductivity is determined from the steady state with a constant heating output. The specific heat capacity of the sample material is calculated according to the temperature from the data sets relating to the thermal diffusivity and thermal conductivity, which data sets are determined directly and over a large temperature range. Because of the enormous savings in time as compared with the prior art, a large number of different solid bodies can be comprehensively characterized thermally for the first time by means of the invention.
机译:本发明涉及一种用于同时确定与温度有关的热导率,热扩散率和比热容的装置和方法,并且包括用于局部加热待检查固体的热源,局部和按时间顺序高分辨率的线和/或用于沿着样品进行非接触式温度测量的表面检测器,以及冷却回路,该冷却回路具有在样品的下边缘周围流动的冷却液,该冷却液的温度升高和流量是连续测量的。通过所描述的方法由样品的瞬时热状态确定热扩散率,所述样品的瞬时热状态在加热和冷却期间以受控的方式被调节。导热系数是由稳定状态确定的,具有恒定的加热输出。根据温度从与热扩散率和热导率有关的数据集中计算出样品材料的比热容,这些数据集是直接在较大的温度范围内确定的。由于与现有技术相比节省了大量的时间,因此可以借助本发明首次对多种不同的固体进行热综合表征。

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