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EPMA QUANTITATIVE ANALYSIS METHOD

机译:EPMA定量分析方法

摘要

PROBLEM TO BE SOLVED: To provide an EPMA quantitative analysis method capable of securing analysis accuracy while operation time is short, regardless of the skill level of analyzer.;SOLUTION: An EPMA quantitative analysis method comprises: a point analysis step of performing a qualitative analysis of an analysis sample by a point analysis under a basic condition; a step of outputting a mass concentration of an analysis objected element obtained by the point analysis as a semi-quantitative value; a standard sample selection step of selecting at least three standard samples for an analytical curve according to the semi-quantitative value; a plane analysis step of performing a plane analysis of the selected standard samples and the analysis sample under a prescribed condition set according to the semi-quantitative value; an average count number outputting step of outputting an average count number of the objected element in an analytical area for each of the standard samples and the analysis sample on the basis of the result of the plane analysis; a regression equation output step of creating the analytical curve based on the average count number of the standard samples to output a regression equation; and a mass concentration calculation step of substituting the average count number of the analysis sample for the regression equation to calculate a mass concentration.;SELECTED DRAWING: None;COPYRIGHT: (C)2019,JPO&INPIT
机译:要解决的问题:提供一种EPMA定量分析方法,无论分析人员的技术水平如何,都能在操作时间短的情况下确保分析准确性。解决方案:EPMA定量分析方法包括:进行定性分析的点分析步骤在基本条件下通过点分析得到分析样品;输出通过点分析得到的分析对象元素的质量浓度作为半定量值的步骤。标准样品选择步骤,根据所述半定量值,选择至少三个标准样品作为分析曲线;平面分析步骤,在根据所述半定量值设定的规定条件下,对所选择的标准样品和所述分析样品进行平面分析。平均计数数输出步骤,根据平面分析的结果,输出每个标准样品和分析样品在分析区域中目标元素的平均计数数;回归方程式输出步骤,其基于标准样品的平均计数创建分析曲线以输出回归方程式;质量浓度计算步骤;将分析样品的平均计数值代入回归方程,以计算质量浓度。;选图:无;版权:(C)2019,JPO&INPIT

著录项

  • 公开/公告号JP2018163069A

    专利类型

  • 公开/公告日2018-10-18

    原文格式PDF

  • 申请/专利权人 DAIHATSU MOTOR CO LTD;

    申请/专利号JP20170060943

  • 发明设计人 IGAWA DAISUKE;

    申请日2017-03-27

  • 分类号G01N23/225;

  • 国家 JP

  • 入库时间 2022-08-21 13:14:19

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