首页> 外国专利> METHOD OF FORMING LEAD ZIRCONATE TITANATE SINTERED COMPACT LEAD ZIRCONATE TITANATE SINTERED COMPACT AND LEAD ZIRCONATE TITANATE SPUTTERING TARGET

METHOD OF FORMING LEAD ZIRCONATE TITANATE SINTERED COMPACT LEAD ZIRCONATE TITANATE SINTERED COMPACT AND LEAD ZIRCONATE TITANATE SPUTTERING TARGET

机译:铅酸锆钛酸盐烧结体的形成方法铅酸锆钛酸盐烧结体和铅酸钛钛酸盐溅射靶的形成方法

摘要

Disclosed is a method for producing a lead zirconate titanate-based sintered body having a uniform crystal phase and a high density of PbO.;A method for producing a lead zirconate titanate-based sintered body according to the present invention is characterized in that a preliminary sintered body obtained by sintering a raw material powder of lead zirconate titanate mixed in a stoichiometric composition at a temperature of 900 C to 1200 C is prepared, , PbO powder is added to the powder of the pulverized pre-sintered body to prepare an excess of lead mixed powder, and the excess of the lead mixed powder is sintered at a temperature lower than the sintering temperature of the pre-sintered body. By dividing the sintering process into two stages, PbZrO3, PbTiO3, ZrO2, TiO2(For example, 95% or more) of the PZT sintered body consisting only of PZT in the stoichiometric composition in which PbO and other intermediate compounds are not present and PbO 2 in the excess component are obtained.;Sintered product, titanic acid, zircon lead zirconate
机译:本发明公开了一种结晶相均匀且PbO密度高的钛酸锆钛酸铅基烧结体的制造方法。本发明的特征在于,预备品的制备方法如下。制备通过在900℃至1200℃的温度下烧结化学计量组成的钛酸锆钛酸铅的原料粉末而获得的烧结体,将PbO粉末添加到粉碎的预烧结体的粉末中以制备过量的铅混合粉末,并且过量的铅混合粉末在低于预烧结体的烧结温度的温度下烧结。通过将烧结过程分为PbZrO 3 ,PbTiO 3 ,ZrO 2 ,TiO 2 两个阶段(对于例如,在不存在PbO和其他中间化合物且过量成分中的PbO 2的化学计量组成中仅由PZT组成的PZT烧结体的95%以上得到。烧结产物,钛酸,锆石锆铅锆酸盐

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