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Method and system for preparation of highly porous and preferentially-oriented {100} platinum nanowires and thin films
Method and system for preparation of highly porous and preferentially-oriented {100} platinum nanowires and thin films
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机译:制备高度多孔且优先取向的{100}铂纳米线和薄膜的方法和系统
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摘要
A method for preparation of highly porous and preferentially-oriented {100} platinum on a substrate by electrodeposition in a deposition bath, comprising using a deposition potential Edep lower than ERHE+150 mV and an acidified platinum salt solution having a Pt salt concentration less than 5.0 mmole L−1 or, in presence of hydrogen, comprising limiting the concentration of Pt salts in the electrolyte to less than 5.0 mmole L−1 and controlling the temperature of the electrolyte. Preferentially-oriented {100} platinum nanowires and thin films, comprising Pt{100} in a range between about 20 and about 60% and having a roughness factor of at least 50 are produced.
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机译:一种通过在沉积浴中电沉积在基材上制备高度多孔且优先取向的{100}铂的方法,该方法包括使用比E RHE Sub>低的沉积电势E dep Sub> +150 mV和Pt盐浓度小于5.0 mmole L 的酸化铂盐溶液,或在氢气存在下,包括将电解质中Pt盐的浓度限制为小于5.0 mmole L −1 Sup>并控制电解质的温度。产生包括在约20%和约60%之间的范围内的Pt {100}并且具有至少50的粗糙度因子的优选取向的{100}铂纳米线和薄膜。
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