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metal core-oxide shell of the core-shell structure nanoparticles of continuous synthesis method and continuous synthesis apparatus, and core-shell structure nanoparticles

机译:连续合成方法和连续合成装置的核-壳结构纳米颗粒的金属核-氧化物壳和核-壳结构纳米颗粒

摘要

The present invention is not causing the variation or aggregation of the particle size of the nanoparticles, less and an object thereof is to provide a continuous method of synthesizing apparatus, and core-shell structure nano-particles in the process. The present invention relates to metal nanoparticles having a diameter of 1~100nM the flow type reaction tube 3 of the preceding stage including at least one stage of a flow-type reaction tube was continuously synthesized, subsequent flow type reaction comprising at least one stage of a flow-type reaction tube Continuous process for the synthesis of core-shell structure nanoparticles uniformly heated by microwave at least flow-through reaction tube 3 is a continuous process for the synthesis of hydrolyzing core-shell structure nanoparticles oxide precursor in the tube 10, before the latter stage of the flow-through reaction and a pipe 3 and 10, comprises means for uniformly heating at least flow type reaction tube 3 by microwave, flow type reaction tube 3 is the reaction tube for a metallic core synthesis, flow type reaction tube 10 is oxide Continuous synthesis apparatus is a reaction tube for the shell synthesis, and to the core-shell structured nanoparticles synthesized in the continuous synthesis method and / or the continuous synthesizer.
机译:本发明不会引起纳米粒子的粒径的变化或聚集,较少,其目的是提供一种连续的合成装置的方法以及该方法中的核-壳结构纳米粒子。本发明涉及直径为1〜100nM的金属纳米粒子,连续地合成包括至少一个阶段的流动型反应管的前级的流动型反应管3,随后的包括至少一个阶段的流动型反应。 (流式反应管)至少在流通反应管3中被微波均匀加热而连续地合成核-壳结构纳米粒子的连续过程是在管10中水解核-壳结构纳米粒子氧化物前体的连续过程,在流通反应的后期之前,管3和10包括用于通过微波至少均匀加热至少流动型反应管3的装置,流动型反应管3是用于金属芯合成,流动型反应的反应管。管10是氧化物。连续合成装置是用于壳合成的反应管,并且使在连续壳中合成的核-壳结构的纳米粒子非连续合成方法和/或连续合成器。

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