首页> 外国专利> METHOD FOR SYNTHESIZING PRUSSIAN BLUE TYPE COMPLEX NANOPARTICLES, AND PRUSSIAN BLUE TYPE COMPLEX NANOPARTICLES SYNTHESIZED BY THE METHOD

METHOD FOR SYNTHESIZING PRUSSIAN BLUE TYPE COMPLEX NANOPARTICLES, AND PRUSSIAN BLUE TYPE COMPLEX NANOPARTICLES SYNTHESIZED BY THE METHOD

机译:合成普鲁士蓝型复合纳米粒子的方法和用该方法合成的普鲁士蓝型复合纳米粒子

摘要

PROBLEM TO BE SOLVED: To provide a method for synthesizing Prussian blue type complex nanoparticles in which a particle diameter of nanoparticles is made smaller and sufficient yield is secured, and cesium adsorbent with improved cesium adsorption capacity using the nanoparticles.SOLUTION: There is provided a method in which, by using a mixing apparatus of liquid which has two, or three or more inflow ports, and has one, or two or more outflow ports after the inflow ports join in the inside, first solution made of aqueous solution of metal salt containing metal M and second solution made of aqueous solution of salt containing hexa cyano iron ([Fe(CN)]) are severally poured from different inflow ports, mixed in the inside to synthesize Prussian blue type complex nanoparticles. The nanoparticles are synthesized by a method satisfying the following condition a or b. a. Solutions are mixed under a condition that Reynolds number in the mixing apparatus after the first solution is mixed with the second solution is 2000 or more. b. Baffle plates are provided inside the mixing apparatus.
机译:解决的问题:提供一种普鲁士蓝型复合纳米粒子的合成方法,该方法使纳米粒子的粒径变小并确保足够的收率,并且使用该纳米粒子具有改善的铯吸附能力的铯吸附剂。一种方法,其中,通过使用具有两个或三个或三个以上流入孔并且在流入孔汇合到内部之后具有一个或两个或多个流出孔的液体的混合装置,由金属盐水溶液制成的第一溶液从不同的流入口分别倒入含有金属M的第二溶液和含有六氰基铁盐([Fe(CN)]的盐的水溶液制成的第二溶液,在内部混合以合成普鲁士蓝型复合纳米粒子。通过满足以下条件a或b的方法合成纳米颗粒。一种。在将第一溶液与第二溶液混合之后,在混合装置中的溶液的雷诺数为2000以上的条件下混合溶液。 b。挡板设置在混合装置内部。

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