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Method of preparing fullerene derivatives using photoaddition reaction of tertiary -silylamine and fullerene

机译：利用叔硅烷基胺与富勒烯的光加成反应制备富勒烯衍生物的方法

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PURPOSE: A manufacturing method of fullerene derivatives is provided to reduce the reaction time, to have a suitable equivalent ratio, to be able to introduce various functional groups, and to have a high yield of products. CONSTITUTION: A manufacturing method of fullerene derivatives comprises a step of synthesizing fullerene derivatives by reacting with addition of silyl-amines represented by Chemical formula 2 to a compound represented by Chemical formula 1. In Chemical formulas, A is a fullerene derivative selected from substituted or non-substituted C60, C70, C72, C76, C78 or C84; R1, R2 and R3 are, respectively, substituted or non-substituted (C1-30) alkyl, (C6-30) aryl, or (C4-30) heteroaryl; R4 and R5 are, respectively, substituted or non-substituted (C1-30) alkyl, (C6-30) aryl, (C1-30) alkyl substituted with alpha-silyl tertiary amino, or (C4-C30) heteroaryl.

机译：目的：提供一种富勒烯衍生物的制备方法，以减少反应时间，具有合适的当量比，能够引入各种官能团并具有高产率的产物。组成：富勒烯衍生物的制造方法包括以下步骤：通过与化学式2表示的化合物加成化学式2表示的甲硅烷基胺反应，合成富勒烯衍生物。在化学式中，A是选自取代的或未取代的C60，C70，C72，C76，C78或C84; R1，R2和R3分别是取代或未取代的（C1-30）烷基，（C6-30）芳基或（C4-30）杂芳基; R4和R5分别是取代或未取代的（C1-30）烷基，（C6-30）芳基，被α-甲硅烷基叔氨基取代的（C1-30）烷基或（C4-C30）杂芳基。

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公开/公告号KR101373763B1

专利类型
公开/公告日2014-03-14

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申请/专利号KR20120016894
发明设计人 윤웅찬;김경목;박혜정;유현지;
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申请日2012-02-20
分类号C07C7/10;C07C13/64;H01L51/50;H01L31/042;
国家 KR
入库时间 2022-08-21 15:41:22

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