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首页> 外国专利> METHOD OF OBTAINMENT OF DIALKYLDITHIOPHOSPHATES OF ZINC WITH HIGH HYDROLYTIC STABILITY, COMPOSITION, ENSURING HIGH HYDROLYTIC STABILITY OF DIALKYLDITHIOPHOSPHATES OF ZINC

METHOD OF OBTAINMENT OF DIALKYLDITHIOPHOSPHATES OF ZINC WITH HIGH HYDROLYTIC STABILITY, COMPOSITION, ENSURING HIGH HYDROLYTIC STABILITY OF DIALKYLDITHIOPHOSPHATES OF ZINC

机译：具有高水解稳定性，组成的锌的二磷酸二磷酸酯的制备方法，以确保锌的二磷酸二磷酸磷酸酯的高水解稳定性

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FIELD: power engineering.;SUBSTANCE: invention relates to the method for production of an additive to lubricant oils containing zinc dialkyl dithiophosphate (Zn-DADTP). In the proposed method phosphorus pentasulfide interacts with alcohol of the general formula ROH, where R - alkyl radical C3-C10, or a mixture of these alcohols at the temperature of 50-80°C in a flow of an inert gas, with subsequent addition of zinc oxide and mineral oil, with a difference in the fact that at the stage of Zn-DADTP carboxylic acid C8-C24 is added in the amount of 1-10 wt %, and upon completion of the reaction triphenylphosphite is added in the amount of 1-10 wt%, at the same time mineral oil is added in the amount of 1-40 wt%.;EFFECT: proposed method makes it possible to improve hydrolytic stability of additives containing Zn-DADTP to preserve operating characteristics of lubricant oils under long-term operation in high-moisture conditions.;12 tbl, 2 dwg, 14 ex
机译：添加剂的制备方法技术领域本发明涉及用于向包含二烷基二硫代磷酸锌（Zn-DADTP）的润滑油添加添加剂的方法。在提出的方法中，五硫化二磷与通式为ROH的醇相互作用，其中R-烷基C 3 -C 10 或这些醇的混合物在50-80°C在惰性气体流中，随后添加氧化锌和矿物油，不同之处在于在Zn-DADTP羧酸阶段C 8 -C 24 的添加量为1-10 wt％，反应完成后，亚磷酸三苯酯的添加量为1-10 wt％，同时矿物油的添加量为1-10 wt％。效果：达到1-40 wt％。效果：所提出的方法可以改善含Zn-DADTP的添加剂的水解稳定性，以在高湿度条件下长期运行时保持润滑油的运行特性。; 12 tbl，2 dwg， 14前

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