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PROCESSING METHOD OF LITHIUM IRON PHOSPHATE USED AS POSITIVE ELECTRODE MATERIAL OF LITHIUM ION BATTERY

机译:锂离子电池正极材料磷酸铁锂的制备方法

摘要

A processing method of lithium iron phosphate used as the positive electrode material of a lithium ion battery comprises: 1) wet-treating the lithium iron phosphate material, i.e. processing the lithium iron phosphate material with a wetting agent of 0.1-3% wt. in concentration, to obtain a homogeneous aqueous suspension of lithium iron phosphate material; 2) leaching high active iron ions on the surface of the lithium iron phosphate material with acid solution, i.e. adding an acid solution with pH value of 0-1 into the suspension of lithium iron phosphate under agitation, to keep the pH value of the obtained solution at the range between 1.5-2.5, while rendering a complete reaction by agitating; 3) filtering and drying, i.e. filtering the solution, washing the filtered lithium iron phosphate with distilled water or pure water, and drying the washed lithium iron phosphate material under vacuum condition or protective gas atmosphere to obtain the finished lithium iron phosphate material. The lithium iron phosphate material is carbon coated. The shelf life and high temperature property of the battery can be improved by the method.
机译:用作锂离子电池的正极材料的磷酸铁锂的处理方法包括:1)湿处理磷酸铁锂材料,即用0.1-3%wt的润湿剂处理磷酸铁锂材料。浓缩得到磷酸锂铁材料的均匀水悬浮液。 2)用酸溶液在磷酸铁锂材料的表面上浸出高活性铁离子,即在搅拌下向磷酸铁锂悬浮液中加入pH值为0-1的酸溶液,以保持所得的pH值。溶液在1.5-2.5之间的范围内,同时通过搅拌使反应完全。 3)过滤并干燥,即过滤溶液,用蒸馏水或纯水洗涤过滤后的磷酸铁锂材料,并在真空条件或保护性气体气氛下干燥洗涤后的磷酸铁锂材料,得到成品的磷酸铁锂材料。磷酸锂铁材料涂有碳。通过该方法可以改善电池的保存期限和高温性能。

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