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Analytical tools and near infrared spectroscopy methods for near infrared spectroscopy

机译:用于近红外光谱的分析工具和近红外光谱方法

摘要

PROBLEM TO BE SOLVED: To provide an analytical tool for near infrared spectroscopic analysis and an analytical method for facilitating cleaning by having a large aperture area for housing a sample aqueous solution and inexpensive by preventing rises in measurement costs.;SOLUTION: A measuring unit 3 is used for irradiating infrared rays to a solid sample and measuring their regularly reflected light. A miniature test tube 6 housing a sample aqueous solution is vertically raised in a test tube stand 9 on a sample base 4. In other words, the sample aqueous solution 7 is housed in the miniature test tube 6 having an inner diameter between 2-5 mm, and a cylindrical SUS reflector 8 for setting an optical path length is submerged in the sample aqueous solution 7. Near infrared rays to be irradiated from a light-emitting part diagonally below on the left side are transmitted through bottom-wall glass of the miniature test tube 6, made incident into the sample aqueous solution 7, reflected into the sample aqueous solution 7 by the cylindrical SUS reflector 8, transmitted through the bottom-wall glass of the miniature test tube 6, received by a light-receiving part diagonally below on the right side, and transmitted through the sample aqueous solution 7 having a set optical path length to obtain an absorption spectrum of the near infrared rays.;COPYRIGHT: (C)2010,JPO&INPIT
机译:解决的问题:提供一种用于近红外光谱分析的分析工具和一种分析方法,该方法具有大的用于容纳样品水溶液的开孔面积,并且通过防止测量成本的增加而廉价进行清洁;解决方案:测量单元3用于将红外线照射到固体样品上并测量其正反射光。容纳样品水溶液的微型试管6在样品基座4上的试管架9中竖直地升高。换言之,将样品水溶液7容纳在内径在2-5之间的微型试管6中。并且,在试样水溶液7中浸没有用于设定光程长度的圆筒形的SUS反射镜8。在该试样水溶液7中浸入有从左侧的斜下方的发光部射出的近红外线。微型试管6入射到样品水溶液7中,通过圆筒形的SUS反射器8反射到样品水溶液7中,该微型试管6通过微型试管6的底壁玻璃,并斜向地由受光部接收。右下方,并通过具有设定光程长度的样品水溶液7透射,以获得近红外线的吸收光谱。版权所有:(C)2010,JPO&INPIT

著录项

  • 公开/公告号JP4950947B2

    专利类型

  • 公开/公告日2012-06-13

    原文格式PDF

  • 申请/专利权人 日本分光株式会社;

    申请/专利号JP20080150637

  • 发明设计人 神 ちひろ;

    申请日2008-06-09

  • 分类号G01N21/01;G01N21/35;

  • 国家 JP

  • 入库时间 2022-08-21 17:40:24

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