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METHOD FOR THE SYNTHESIS AND PURIFICATION FOR ADAMANTANE DIOL FROM ADAMANTANE WHICH CAN OBTAIN ADAMANTANE-1,3-DIOL AND ADAMANTANE-1-OL AT HIGH PURITY
METHOD FOR THE SYNTHESIS AND PURIFICATION FOR ADAMANTANE DIOL FROM ADAMANTANE WHICH CAN OBTAIN ADAMANTANE-1,3-DIOL AND ADAMANTANE-1-OL AT HIGH PURITY
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机译:可以高纯度获得金刚烷-1,3-二醇和金刚烷-1-OL的金刚烷合成和纯化金刚烷二酚的方法
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摘要
PURPOSE: A method for the synthesis and purification for adamantane diol from adamantine is provided to selectively synthesize adamantane-1,3-diol and adamantane-1-ol at high purity through the hydroxy reaction of adamantine using a composite co-catalyst for a short reaction time.;CONSTITUTION: A method for the synthesis and purification for adamantane diol from adamantine comprises a step of contacting an adamantine compound with oxygen in the presence of N-hydroxyphthalimide and cocatalyst. The cocatalyst is one or more composite cocatalysts selected from the group consisting of oxides including elements selected from Co, Mn, V and Ru, inorganic acid salts, inorganic acid salts, halide, complexes, heteropolyacids, and heteropolyacid salts.;COPYRIGHT KIPO 2012
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