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Fabrication of high performance densified nanocrystalline bulk thermoelectric materials using high pressure sintering technique
Fabrication of high performance densified nanocrystalline bulk thermoelectric materials using high pressure sintering technique
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机译:利用高压烧结技术制备高性能致密纳米晶块状热电材料
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摘要
The present invention provides a method for the fabrication of high performance densified nanocrystalline bulk thermoelectric material, comprising: (1) preparing a thermoelectric alloy nanopowders by a ball milling process to achieve an average crystal size of 5 -30 nm, and (2) preparing the nanocrystalline bulk thermoelectric material by high pressure sintering at a temperature of 0.25 - 0.8Tm under a pressure of 0.8 - 6.0 GPa for 10 - 120 minutes, to achieve a relative density of 90 - 100 % and an average grain size of 10 - 50 nm. The method is easy to operate and allows the production of a thermoelectric material with a ZT value higher than 2. In addition, the method can ensure both good thermoelectric properties and high density, and therefore have important applications for energy industry.
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