首页> 外国专利> Surface engineered nanoparticles for improved surface enhanced Raman scattering applications and method for preparing same

Surface engineered nanoparticles for improved surface enhanced Raman scattering applications and method for preparing same

机译:用于改进的表面增强拉曼散射应用的表面工程纳米粒子及其制备方法

摘要

A method for producing metal nanoparticles that when associated with an analyte material will generate an amplified SERS spectrum when the analyte material is illuminated by a light source and a spectrum is recorded. The method for preparing the metal nanoparticles comprises the steps of (i) forming a water-in-oil microemulsion comprising a bulk oil phase, a dilute water phase, and one or more surfactants, wherein the water phase comprises a transition metal ion; (ii) adding an aqueous solution comprising a mild reducing agent to the water-in-oil microemulsion; (iii) stirring the water-in-oil microemulsion and aqueous solution to initiate a reduction reaction resulting in the formation of a fine precipitate dispersed in the water-in-oil microemulsion; and (iv) separating the precipitate from the water-in-oil microemulsion.
机译:一种用于生产金属纳米颗粒的方法,当与分析物材料结合时,当通过光源照射分析物材料并记录光谱时,该金属纳米颗粒将产生放大的SERS光谱。制备金属纳米粒子的方法包括以下步骤:(i)形成油包水微乳液,其包含本体油相,稀水相和一种或多种表面活性剂,其中水相包含过渡金属离子; (ii)向油包水微乳液中加入包含温和还原剂的水溶液; (iii)搅拌油包水微乳液和水溶液以引发还原反应,从而形成分散在油包水微乳液中的细小沉淀物; (iv)从油包水型微乳中分离出沉淀物。

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