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Surface engineered nanoparticles for improved surface enhanced Raman scattering applications and method for preparing same
Surface engineered nanoparticles for improved surface enhanced Raman scattering applications and method for preparing same
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机译:用于改进的表面增强拉曼散射应用的表面工程纳米粒子及其制备方法
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摘要
A method for producing metal nanoparticles that when associated with an analyte material will generate an amplified SERS spectrum when the analyte material is illuminated by a light source and a spectrum is recorded. The method for preparing the metal nanoparticles comprises the steps of (i) forming a water-in-oil microemulsion comprising a bulk oil phase, a dilute water phase, and one or more surfactants, wherein the water phase comprises a transition metal ion; (ii) adding an aqueous solution comprising a mild reducing agent to the water-in-oil microemulsion; (iii) stirring the water-in-oil microemulsion and aqueous solution to initiate a reduction reaction resulting in the formation of a fine precipitate dispersed in the water-in-oil microemulsion; and (iv) separating the precipitate from the water-in-oil microemulsion.
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