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PROCEDURES FOR THE RECOVERY OF EASTERN AND/OR EASTERN EDUCATIONAL WATERS

机译:东部和/或东部教育水域的恢复程序

摘要

Process for the preparation of a compound of general formula (II) wherein R1 and R2 independently are hydrogen or a hydroxy- or hydrocarbyl group; or wherein R1 and R2 together are a double bonded oxygen; R3 is hydrogen; R4 is a nitrobenzophenone group; and R5 and R6 independently are hydrogen or a hydroxy- or hydrocarbyl group; from a compound of general formula (I) wherein, R1, R2 R3, R5 and R6 are as defined above and R4 is hydrogen; wherein the compound of formula (I) is reacted under alkaline conditions with 2-chloro-5-nitrobenzophenone in the presence of an alkanolic solvent and the compound of formula (II) is directly crystallized from this alkanolic solvent. Complex of an alkanol and a compound of general formula (II) obtainable from the above process and processes wherein the above process or complex are used.
机译:制备通式(Ⅱ)化合物的方法,其中R 1和R 2独立地是氢或羟基或烃基。或其中R1和R2一起是双键氧;或R3是氢; R4是硝基二苯甲酮基团; R5和R6独立地是氢或羟基或烃基;通式(I)的化合物,其中R 1,R 2,R 3,R 5和R 6如上定义,R 4为氢;其中式(Ⅰ)化合物在碱性条件下在链烷醇溶剂存在下与2-氯-5-硝基二苯甲酮反应,式(Ⅱ)化合物直接从该链烷醇溶剂中结晶。可通过上述方法获得的链烷醇和通式(II)化合物的配合物,其中使用了上述方法或配合物。

著录项

  • 公开/公告号DE602005008997D1

    专利类型

  • 公开/公告日2008-09-25

    原文格式PDF

  • 申请/专利权人 N.V. ORGANON;

    申请/专利号DE20056008997T

  • 发明设计人 WILLEMS L.G.M.;MAAS H.J.F.;OSTENDORF M.;

    申请日2005-08-22

  • 分类号C07J1;

  • 国家 DE

  • 入库时间 2022-08-21 19:47:59

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