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Device for execution of rectification with blended chemical reaction, comprises rectifying column including reactive- and separating column that are connected by a central container and a bypass parallel to the central container
Device for execution of rectification with blended chemical reaction, comprises rectifying column including reactive- and separating column that are connected by a central container and a bypass parallel to the central container
The device for carrying out rectification with blended chemical reaction, comprises coupled rectifying columns comprising reactive column (3A)- and separating column (2A) that are connected by a central container (1A) and a bypass (4A) parallel to the central container. The central container is connected with the reactive column via pipelines, by which a part of the contents of the container is suppliable into the reactive column. The central container is connected with the separating column via a supply- or drainpipe. The device is operated in a semi-discontinuous manner. The device for carrying out rectification with blended chemical reaction, comprises coupled rectifying columns comprising reactive column (3A)- and separating column (2A) that are connected by a central container (1A) and a bypass (4A) parallel to the central container. The central container is connected with the reactive column via pipelines, by which a part of the contents of the container is suppliable into the reactive column. The central container is connected with the separating column via a supply- or drainpipe. A part of contents of the separating column is suppliable into the central container via the drainpipe and a part of contents of the central container is suppliable into the separating column via the supply pipe. The bypass allows a material flow in a direction and the material flow in the bypass of the reactive column is led into the separating column. An educt is supplied via a feed line (7A) at the head or at the sump of the reactive column. The feed line of the educt exhibits a heat exchanger for heating the educt. The head of the reactive column is coupled with the sump of the separating column by a flow connection. The central container is connected with the sump of the reactive column via the pipelines, is connected with the head of the separating column by the supply pipe and the drainpipe, and is connected with the sump of the separating column by the supply pipe and the drainpipe. The sump of the reactive column is connected with the head of the separating column by a flow connection. The rectification column exhibits a reflux with a condenser and/or reboiler. An independent claim is included for a procedure for carrying out the rectification with blended chemical reaction.
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